2,6-bis-trifluoromethylobenzoic acid 2-[1-(ethoxycabonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester

Base Information

Chemical Name:2,6-bis-trifluoromethylobenzoic acid 2-[1-(ethoxycabonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester
CAS No.:1371607-57-6
Molecular Formula:C₂₃H₂₆F₆N₂O₆
Molecular Weight:540.46
Hs Code.:

Synonyms:2,6-bis-trifluoromethylobenzoic acid 2-[1-(ethoxycabonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,6-bis-trifluoromethylobenzoic acid 2-[1-(ethoxycabonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester

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Technology Process of 2,6-bis-trifluoromethylobenzoic acid 2-[1-(ethoxycabonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester

There total 2 articles about 2,6-bis-trifluoromethylobenzoic acid 2-[1-(ethoxycabonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 1353048-90-4
2,6-bis(trifluoromethyl)benzoic acid cesium salt

: 1371607-59-8
(S)-ethyl-2-(2-(2-(bromomethyl)acrylamido)-4-methylpentaneamido)acetate

: 1371607-57-6
2,6-bis-trifluoromethylobenzoic acid 2-[1-(ethoxycabonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester

Guidance literature:: In acetone; for 2h; Reflux;

Reference yield:

: 1598420-58-6
ethyl 2-[2-{2-(bromomethyl)-N-(1-{2,4-dimethoxyphenyl}ethyl)acrylamido}-4-methylpentanamido]acetate

: 1371607-57-6
2,6-bis-trifluoromethylobenzoic acid 2-[1-(ethoxycabonylmethylcarbamoyl)-3-methylbutylcarbamoyl]allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 20 °C

2: acetone / 2 h / Reflux

With trifluoroacetic acid; In dichloromethane; acetone;
DOI:10.1016/j.tetasy.2014.01.016