([2-5,10,15,20-tetrakis(trifluoromethyl)porphinato]zinc(II))-[(5'-10',20'-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)]ethyne

Base Information

Chemical Name:([2-5,10,15,20-tetrakis(trifluoromethyl)porphinato]zinc(II))-[(5'-10',20'-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)]ethyne
CAS No.:424788-30-7
Molecular Formula:C₇₀H₅₀F₁₂N₈O₄Zn₂
Molecular Weight:1425.98
Hs Code.:

Synonyms:([2-5,10,15,20-tetrakis(trifluoromethyl)porphinato]zinc(II))-[(5'-10',20'-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)]ethyne

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Chemical Property of ([2-5,10,15,20-tetrakis(trifluoromethyl)porphinato]zinc(II))-[(5'-10',20'-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)]ethyne

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Technology Process of ([2-5,10,15,20-tetrakis(trifluoromethyl)porphinato]zinc(II))-[(5'-10',20'-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)]ethyne

There total 1 articles about ([2-5,10,15,20-tetrakis(trifluoromethyl)porphinato]zinc(II))-[(5'-10',20'-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)]ethyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 402508-67-2
(5-ethynyl-10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)

: 310408-38-9
[2-bromo-5,10,15,20-tetrakis(trifluoromethyl)porphyrinato]zinc(II)

: 424788-30-7
([2-5,10,15,20-tetrakis(trifluoromethyl)porphinato]zinc(II))-[(5'-10',20'-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)]ethyne

Guidance literature:: With As(C₆H₅)3; (C₂H₅)3N; Pd₂(C₆H₅CHCHCOCHCHC₆H₅)3; In tetrahydrofuran; triethylamine; under N2; Zn complexes, Pd complex and As(C6H5)3 were dissolved in THF/triethylamine (5/1), mixt. was stirred for 20 h at 40°C; solvent was evapd., residue was chromd. (silica gel, hexanes/THF (3/1)) followed by (SX-1 biobeads, THF);
DOI:10.1021/ja012489h