?2-(3-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-6-oxo-6H-xanthen-9-yl)benzoic acid

Base Information

Chemical Name:?2-(3-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-6-oxo-6H-xanthen-9-yl)benzoic acid
CAS No.:1398063-67-6
Molecular Formula:C₂₈H₁₈O₆
Molecular Weight:450.447
Hs Code.:

Synonyms:?2-(3-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-6-oxo-6H-xanthen-9-yl)benzoic acid

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Chemical Property of ?2-(3-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-6-oxo-6H-xanthen-9-yl)benzoic acid

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Technology Process of ?2-(3-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-6-oxo-6H-xanthen-9-yl)benzoic acid

There total 2 articles about ?2-(3-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-6-oxo-6H-xanthen-9-yl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1398063-62-1
fluorescein monotrifluoromethanesulfonate

: 164014-95-3
2.3-dihydro-1,4-benzodioxin-6-ylboronic acid

: 1398063-67-6
?2-(3-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-6-oxo-6H-xanthen-9-yl)benzoic acid

Guidance literature:: With palladium diacetate; potassium carbonate; triphenylphosphine; In 1,4-dioxane; water; at 120 ℃; for 0.5h; Microwave irradiation;
DOI:10.1016/j.bmcl.2012.07.101

Reference yield:

: 518-45-6
fluorescein free acid

: 1398063-67-6
?2-(3-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-6-oxo-6H-xanthen-9-yl)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 80 °C / Microwave irradiation

2: palladium diacetate; triphenylphosphine; potassium carbonate / 1,4-dioxane; water / 0.5 h / 120 °C / Microwave irradiation

With palladium diacetate; potassium carbonate; triphenylphosphine; In 1,4-dioxane; water; N,N-dimethyl-formamide; 2: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.bmcl.2012.07.101