Thiocarbonic acid O-benzyl ester S-{(R)-2-benzyloxycarbonylamino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyl} ester

Base Information

• Chemical Name: Thiocarbonic acid O-benzyl ester S-{(R)-2-benzyloxycarbonylamino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyl} ester
• CAS No.: 126380-86-7
• Molecular Formula: C₂₃H₂₇Cl₂N₃O₅S
• Molecular Weight: 528.456

Synonyms:Thiocarbonic acid O-benzyl ester S-{(R)-2-benzyloxycarbonylamino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyl} ester

Chemical Property of Thiocarbonic acid O-benzyl ester S-{(R)-2-benzyloxycarbonylamino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyl} ester

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Technology Process of Thiocarbonic acid O-benzyl ester S-{(R)-2-benzyloxycarbonylamino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyl} ester

There total 1 articles about Thiocarbonic acid O-benzyl ester S-{(R)-2-benzyloxycarbonylamino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyl} ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.2%

1,1-bis-(2-chloroethyl)-hydrazine (10487-06-6) + N,S-dicarbobenzoxy-L-cysteine (57912-35-3) → Thiocarbonic acid O-benzyl ester S-{(R)-2-benzyloxycarbonylamino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyl} ester (126380-86-7)

Guidance literature:

With dicyclohexyl-carbodiimide; In chloroform; 1) 0 degC, 4 h; 2) 1 h, room temp.;

Reference yield: 89.0%

Thiocarbonic acid O-benzyl ester S-{(R)-2-benzyloxycarbonylamino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyl} ester (126380-86-7) → Thiocarbonic acid S-{(R)-2-amino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyl} ester O-benzyl ester; hydrobromide (126333-94-6)

Guidance literature:

With hydrogen bromide; In acetic acid; for 1h; Ambient temperature;

upstream raw materials:

1,1-bis-(2-chloroethyl)-hydrazine

N,S-dicarbobenzoxy-L-cysteine

Downstream raw materials:

Thiocarbonic acid S-{(R)-2-amino-2-[N',N'-bis-(2-chloro-ethyl)-hydrazinocarbonyl]-ethyl} ester O-benzyl ester; hydrobromide

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