6'-PNZ-2',3,3''-triBoc-1-(N-phthalimido-2-amino-ethylsulfonamide)-sisomicin

Base Information

Chemical Name:6'-PNZ-2',3,3''-triBoc-1-(N-phthalimido-2-amino-ethylsulfonamide)-sisomicin
CAS No.:1154759-28-0
Molecular Formula:C₅₂H₇₃N₇O₂₁S
Molecular Weight:1164.25
Hs Code.:

Synonyms:6'-PNZ-2',3,3''-triBoc-1-(N-phthalimido-2-amino-ethylsulfonamide)-sisomicin

Suppliers and Price of 6'-PNZ-2',3,3''-triBoc-1-(N-phthalimido-2-amino-ethylsulfonamide)-sisomicin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 6'-PNZ-2',3,3''-triBoc-1-(N-phthalimido-2-amino-ethylsulfonamide)-sisomicin

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 6'-PNZ-2',3,3''-triBoc-1-(N-phthalimido-2-amino-ethylsulfonamide)-sisomicin

There total 11 articles about 6'-PNZ-2',3,3''-triBoc-1-(N-phthalimido-2-amino-ethylsulfonamide)-sisomicin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1154758-59-4
6'-PNZ-2',3,3''-triBoc-sisomicin

: 4403-36-5
2-phthalimido-ethanesulfonyl chloride

: 1154759-28-0
6'-PNZ-2',3,3''-triBoc-1-(N-phthalimido-2-amino-ethylsulfonamide)-sisomicin

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1154759-28-0
6'-PNZ-2',3,3''-triBoc-1-(N-phthalimido-2-amino-ethylsulfonamide)-sisomicin

Guidance literature:: Multi-step reaction with 3 steps

1: 4-methyl-morpholine / tetrahydrofuran / 3 h

2: 2,2',2''-triaminotriethylamine / dichloromethane / 0.75 h

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

With 4-methyl-morpholine; 2,2',2''-triaminotriethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 32385-11-8
sisomicin

: 1154759-28-0
6'-PNZ-2',3,3''-triBoc-1-(N-phthalimido-2-amino-ethylsulfonamide)-sisomicin

Guidance literature:: Multi-step reaction with 6 steps

1: zinc diacetate / methanol; dichloromethane

2: zinc diacetate; triethylamine / tetrahydrofuran; methanol

3: tetrahydrofuran / 2.5 h

4: 4-methyl-morpholine / tetrahydrofuran / 3 h

5: 2,2',2''-triaminotriethylamine / dichloromethane / 0.75 h

6: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

With 4-methyl-morpholine; 2,2',2''-triaminotriethylamine; zinc diacetate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane;