1-((2-(3-chlorophenyl)-4-methylthiazol-5-yl)methylene) thiosemicarbazide

Base Information

Chemical Name:1-((2-(3-chlorophenyl)-4-methylthiazol-5-yl)methylene) thiosemicarbazide
CAS No.:1453840-19-1
Molecular Formula:C₁₂H₁₁ClN₄S₂
Molecular Weight:310.831
Hs Code.:

Synonyms:1-((2-(3-chlorophenyl)-4-methylthiazol-5-yl)methylene) thiosemicarbazide

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Chemical Property of 1-((2-(3-chlorophenyl)-4-methylthiazol-5-yl)methylene) thiosemicarbazide

Chemical Property:

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Technology Process of 1-((2-(3-chlorophenyl)-4-methylthiazol-5-yl)methylene) thiosemicarbazide

There total 3 articles about 1-((2-(3-chlorophenyl)-4-methylthiazol-5-yl)methylene) thiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1206971-37-0
2-(3-chlorophenyl)-4-methylthiazole-5-carbaldehyde

: 79-19-6
thiosemicarbazide

: 1453840-19-1
1-((2-(3-chlorophenyl)-4-methylthiazol-5-yl)methylene) thiosemicarbazide

Guidance literature:: In methanol; for 2h;
DOI:10.1080/10426507.2012.745542

Reference yield:

: 1160573-81-8
ethyl 2-(3-chlorophenyl)-4-methylthiazole-5-carboxylate

: 1453840-19-1
1-((2-(3-chlorophenyl)-4-methylthiazol-5-yl)methylene) thiosemicarbazide

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / diethyl ether / 1.5 h / 0 °C

2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 20 °C

3: methanol / 2 h

With lithium aluminium tetrahydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In methanol; diethyl ether; dimethyl sulfoxide;
DOI:10.1080/10426507.2012.745542

Reference yield:

: 1181778-82-4
(2-(3-chlorophenyl)-4-methylthiazol-5-yl)methanol

: 1453840-19-1
1-((2-(3-chlorophenyl)-4-methylthiazol-5-yl)methylene) thiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 20 °C

2: methanol / 2 h

With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In methanol; dimethyl sulfoxide;
DOI:10.1080/10426507.2012.745542