C₅₄H₇₂O₈

Base Information

Chemical Name:C₅₄H₇₂O₈
CAS No.:1354747-48-0
Molecular Formula:C₅₄H₇₂O₈
Molecular Weight:849.161
Hs Code.:

C<sub>54</sub>H<sub>72</sub>O<sub>8</sub>

Synonyms:C₅₄H₇₂O₈

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Chemical Property of C₅₄H₇₂O₈

Chemical Property:

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Technology Process of C₅₄H₇₂O₈

There total 17 articles about C₅₄H₇₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1354747-47-9
C₂₅H₄₀O₂

: 1354747-45-7
C₃₁H₃₆O₆

: 1354747-48-0
C₅₄H₇₂O₈

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; for 2h; optical yield given as %de; diastereoselective reaction; Inert atmosphere; Reflux;
DOI:10.1021/ol2032448

Reference yield:

: 201279-58-5
1-deoxy-1-allyl-2,3,4,6-tetra-O-acetyl-D-galactopyranoside

: 1354747-48-0
C₅₄H₇₂O₈

Guidance literature:: Multi-step reaction with 11 steps

1.1: methanol; sodium methylate / 1 h / 20 °C / Inert atmosphere

2.1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

5.2: 0 - 20 °C / Inert atmosphere

6.1: tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; 2-phenyl-1,4-benzoquinone / dichloromethane / 0.08 h / 55 °C / Inert atmosphere; Molecular sieve

6.2: 48 h / 55 °C / Inert atmosphere; Molecular sieve

7.1: sodium methylate / methanol / 2 h / 20 °C / Inert atmosphere

7.2: 20 °C / Inert atmosphere

8.1: titanium(IV) isopropylate; L-(+)-diisopropyl tartrate / dichloromethane / 0.75 h / -40 °C / Inert atmosphere; Molecular sieve

8.2: 24 h / -40 - -20 °C / Inert atmosphere

9.1: 1H-imidazole; iodine; triphenylphosphine / diethyl ether; benzene / 0.67 h / 20 °C / Inert atmosphere

10.1: zinc / ethanol / 0.75 h / Inert atmosphere; Reflux

11.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / Inert atmosphere; Reflux

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; titanium(IV) isopropylate; methanol; tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); L-(+)-diisopropyl tartrate; tetrabutyl ammonium fluoride; iodine; sodium methylate; sodium hydride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 2-phenyl-1,4-benzoquinone; zinc; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; mineral oil; benzene; 8.1: Sharpless epoxidation / 8.2: Sharpless epoxidation;
DOI:10.1021/ol2032448

Reference yield:

: 1354747-41-3
C₃₁H₃₆O₅

: 1354747-48-0
C₅₄H₇₂O₈

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; 2-phenyl-1,4-benzoquinone / dichloromethane / 0.08 h / 55 °C / Inert atmosphere; Molecular sieve

1.2: 48 h / 55 °C / Inert atmosphere; Molecular sieve

2.1: sodium methylate / methanol / 2 h / 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: titanium(IV) isopropylate; L-(+)-diisopropyl tartrate / dichloromethane / 0.75 h / -40 °C / Inert atmosphere; Molecular sieve

3.2: 24 h / -40 - -20 °C / Inert atmosphere

4.1: 1H-imidazole; iodine; triphenylphosphine / diethyl ether; benzene / 0.67 h / 20 °C / Inert atmosphere

5.1: zinc / ethanol / 0.75 h / Inert atmosphere; Reflux

6.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / Inert atmosphere; Reflux

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; titanium(IV) isopropylate; tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); L-(+)-diisopropyl tartrate; iodine; sodium methylate; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 2-phenyl-1,4-benzoquinone; zinc; In methanol; diethyl ether; ethanol; dichloromethane; benzene; 3.1: Sharpless epoxidation / 3.2: Sharpless epoxidation;
DOI:10.1021/ol2032448