4-nitrophenyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1→6)-2,3-O-isopropylidene-α-Dmannopyranoside

Base Information

Chemical Name:4-nitrophenyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1→6)-2,3-O-isopropylidene-α-Dmannopyranoside
CAS No.:1628187-19-8
Molecular Formula:C₄₉H₄₅NO₁₇
Molecular Weight:919.893
Hs Code.:

Synonyms:4-nitrophenyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1→6)-2,3-O-isopropylidene-α-Dmannopyranoside

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Chemical Property of 4-nitrophenyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1→6)-2,3-O-isopropylidene-α-Dmannopyranoside

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Technology Process of 4-nitrophenyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1→6)-2,3-O-isopropylidene-α-Dmannopyranoside

There total 2 articles about 4-nitrophenyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1→6)-2,3-O-isopropylidene-α-Dmannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: C₃₆H₂₈Cl₃NO₁₀

: p-nitrophenyl 2,3-O-isopropylidene-α-D-mannopyranoside

: 1628187-19-8
4-nitrophenyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1→6)-2,3-O-isopropylidene-α-Dmannopyranoside

Guidance literature:: C₃₆H₂₈Cl₃NO₁₀; p-nitrophenyl 2,3-O-isopropylidene-α-D-mannopyranoside; In dichloromethane; for 0.5h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; for 2h;
DOI:10.3390/molecules19056683

Reference yield:

: 10357-27-4
4-nitrophenyl-α-D-mannopyranoside

: 1628187-19-8
4-nitrophenyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1→6)-2,3-O-isopropylidene-α-Dmannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 2 h / 70 °C / Inert atmosphere

2.1: dichloromethane / 0.5 h / Molecular sieve; Inert atmosphere

2.2: 2 h

With toluene-4-sulfonic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.3390/molecules19056683