1,3-dimethoxy-5-heptadecylbenzene

Base Information

• Chemical Name: 1,3-dimethoxy-5-heptadecylbenzene
• CAS No.: 41395-17-9
• Molecular Formula: C₂₅H₄₄O₂
• Molecular Weight: 376.623
• Mol file: 41395-17-9.mol

Synonyms:1,3-dimethoxy-5-heptadecylbenzene

Chemical Property of 1,3-dimethoxy-5-heptadecylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-dimethoxy-5-heptadecylbenzene

There total 9 articles about 1,3-dimethoxy-5-heptadecylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

1,3-dimethoxy-5-(heptadec-1-enyl)benzene → 1,3-dimethoxy-5-heptadecylbenzene (41395-17-9)

Guidance literature:

With 10% Pd/C; hydrogen; In methanol; chloroform; at 20 ℃; for 24h;

DOI:10.1021/jf302872a

Reference yield: 45.0%

1-(3',5'-Dimethoxyphenyl)heptadecan-1-ol (52483-25-7) → 1,3-dimethoxy-5-heptadecylbenzene (41395-17-9)

Guidance literature:

With triethylsilane; In trifluoroacetic acid; at 45 ℃; for 24h;

DOI:10.1248/cpb.37.2431

Reference yield:

hexadecylmagnesium bromide (872-26-4) → 1,3-dimethoxy-5-heptadecylbenzene (41395-17-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 62 percent / tetrahydrofuran / -20 - 20 °C

2: 69 percent / 2N KOH / 2 h / Heating

3: 45 percent / Et₃SiH / trifluoroacetic acid / 24 h / 45 °C

With triethylsilane; potassium hydroxide; In tetrahydrofuran; trifluoroacetic acid;

DOI:10.1248/cpb.37.2431

upstream raw materials:

1-(3,4,5-trimethoxy-phenyl)-heptadecan-1-one

1-(3',5'-Dimethoxyphenyl)heptadecan-1-ol

hexadecylmagnesium bromide

3,5-dimethoxybenzoyl chloride

Downstream raw materials:

2-heptadecyl-4,6-dimethoxy-benzaldehyde

5-heptadecylresorcinol

2-heptadecyl-4,6-dimethoxy-3-methyl-benzaldehyde

1-heptadecyl-3,5-dimethoxy-2-methyl-benzene