Technology Process of C29H30N2O5
There total 9 articles about C29H30N2O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
di-isopropyl azodicarboxylate; triphenylphosphine;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere
1.2: 145 °C / Inert atmosphere
2.1: potassium hydroxide / water / 4 h / Inert atmosphere; Reflux
3.1: pyridine; p-toluenesulfonyl chloride / 4 h / 20 °C / Inert atmosphere
4.1: boron tribromide / dichloromethane / 4 h / 20 °C
4.2: 16 h / 0 - 20 °C
5.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
With
pyridine; di-isopropyl azodicarboxylate; boron tribromide; sodium hydride; p-toluenesulfonyl chloride; triphenylphosphine; potassium hydroxide;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
5.1: Mitsunobu reaction;
DOI:10.1039/c2ob00022a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridine; p-toluenesulfonyl chloride / 4 h / 20 °C / Inert atmosphere
2.1: boron tribromide / dichloromethane / 4 h / 20 °C
2.2: 16 h / 0 - 20 °C
3.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
With
pyridine; di-isopropyl azodicarboxylate; boron tribromide; p-toluenesulfonyl chloride; triphenylphosphine;
In
tetrahydrofuran; dichloromethane;
3.1: Mitsunobu reaction;
DOI:10.1039/c2ob00022a
