benzyl N-chloroacetyl-N₂-(2-fluorenylmethoxycarbonyl)aminoethylglycinate

Base Information

• Chemical Name: benzyl N-chloroacetyl-N₂-(2-fluorenylmethoxycarbonyl)aminoethylglycinate
• CAS No.: 1292200-63-5
• Molecular Formula: C₂₈H₂₇ClN₂O₅
• Molecular Weight: 506.986
• Mol file: 1292200-63-5.mol

Synonyms:benzyl N-chloroacetyl-N₂-(2-fluorenylmethoxycarbonyl)aminoethylglycinate

Chemical Property of benzyl N-chloroacetyl-N₂-(2-fluorenylmethoxycarbonyl)aminoethylglycinate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of benzyl N-chloroacetyl-N₂-(2-fluorenylmethoxycarbonyl)aminoethylglycinate

There total 1 articles about benzyl N-chloroacetyl-N₂-(2-fluorenylmethoxycarbonyl)aminoethylglycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

benzyl N-[2-((fluorenylmethoxycarbonyl)amino)ethyl]glycinate (791778-61-5) + chloroacetic acid (79-11-8) → benzyl N-chloroacetyl-N2-(2-fluorenylmethoxycarbonyl)aminoethylglycinate (1292200-63-5)

Guidance literature:

chloroacetic acid; With dicyclohexyl-carbodiimide; In dichloromethane; for 0.5h; Inert atmosphere;

benzyl N-[2-((fluorenylmethoxycarbonyl)amino)ethyl]glycinate; With pyridine; In dichloromethane; for 3h; Inert atmosphere;

DOI:10.1016/j.bmcl.2011.01.130

Reference yield:

benzyl N-chloroacetyl-N2-(2-fluorenylmethoxycarbonyl)aminoethylglycinate (1292200-63-5) → C28H27IN2O5

Guidance literature:

With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; at 20 ℃; for 20h; Inert atmosphere; Darkness;

DOI:10.1016/j.bmcl.2011.01.130

upstream raw materials:

benzyl N-[2-((fluorenylmethoxycarbonyl)amino)ethyl]glycinate

chloroacetic acid