(5R,2E)-methyl 5-(4-methoxyphenyl)-5-(2-thienylsulfonyl)amino-2-pentenoate

Base Information

Chemical Name:(5R,2E)-methyl 5-(4-methoxyphenyl)-5-(2-thienylsulfonyl)amino-2-pentenoate
CAS No.:1068150-72-0
Molecular Formula:C₁₇H₁₉NO₅S₂
Molecular Weight:381.474
Hs Code.:

Synonyms:(5R,2E)-methyl 5-(4-methoxyphenyl)-5-(2-thienylsulfonyl)amino-2-pentenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5R,2E)-methyl 5-(4-methoxyphenyl)-5-(2-thienylsulfonyl)amino-2-pentenoate

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Technology Process of (5R,2E)-methyl 5-(4-methoxyphenyl)-5-(2-thienylsulfonyl)amino-2-pentenoate

There total 1 articles about (5R,2E)-methyl 5-(4-methoxyphenyl)-5-(2-thienylsulfonyl)amino-2-pentenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: N-(4-methoxyphenyl)methylidene 2-thiophenesulfonamide

: 85636-50-6
1-(trimethylsiloxy)-1-methoxy-1,3-butadiene

: 1068150-75-3
C₁₇H₁₉NO₅S₂

: 1068150-72-0
(5R,2E)-methyl 5-(4-methoxyphenyl)-5-(2-thienylsulfonyl)amino-2-pentenoate

Guidance literature:: N-(4-methoxyphenyl)methylidene 2-thiophenesulfonamide; With C₆₈H₆₂Br₂Cu₂Fe₂P₂S₂; silver perchlorate; In dichloromethane; at 20 ℃; for 0.0833333h; Inert atmosphere;

1-(trimethylsiloxy)-1-methoxy-1,3-butadiene; In dichloromethane; at 20 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol8019082

Reference yield: 100.0%

: 1068150-72-0
(5R,2E)-methyl 5-(4-methoxyphenyl)-5-(2-thienylsulfonyl)amino-2-pentenoate

: 1125508-22-6
(R)-methy 5-(4-methoxyphenyl)-5-(2-thienylsulfonylamino)pentanoate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 2h; under 760.051 Torr; Inert atmosphere;
DOI:10.1021/ol8019082