2,3,4,6-tetra-O-acetyl-N--β-D-mannopyranosylamine

Base Information

Chemical Name:2,3,4,6-tetra-O-acetyl-N--β-D-mannopyranosylamine
CAS No.:74761-78-7
Molecular Formula:C₃₀H₃₄N₂O₁₂S₂
Molecular Weight:678.738
Hs Code.:

2,3,4,6-tetra-O-acetyl-N-<N-(benzyloxycarbonyl)-2-(2-thienyl)-L-thiazolidine-4-carbonyl>-β-D-mannopyranosylamine

Synonyms:2,3,4,6-tetra-O-acetyl-N--β-D-mannopyranosylamine

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Chemical Property of 2,3,4,6-tetra-O-acetyl-N--β-D-mannopyranosylamine

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Technology Process of 2,3,4,6-tetra-O-acetyl-N--β-D-mannopyranosylamine

There total 3 articles about 2,3,4,6-tetra-O-acetyl-N--β-D-mannopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 41355-50-4
1-amino-2,3,4,6-tetra-O-acetyl-β-D-mannopyranosyl

: 74761-77-6
N-(benzyloxycarbonyl)-2-(2-thienyl)-L-thiazolidine-4-carboxylic acid

: 74761-78-7
2,3,4,6-tetra-O-acetyl-N--β-D-mannopyranosylamine

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; for 16h;
DOI:10.1016/S0008-6215(00)85529-9

Reference yield:

: 83-87-4,604-68-2,604-69-3,2152-77-4,4026-35-1,4163-59-1,4163-60-4,4163-61-5,4163-65-9,4257-94-7,4257-96-9,16299-15-3,19186-39-1,19189-55-0,25878-60-8,25941-03-1,32445-48-0,32445-49-1,32445-53-7,32445-54-8,34685-58-0,34685-59-1,43168-42-9,43168-44-1,43169-22-8,43169-25-1,66966-07-2,70749-17-6,80184-01-6,93221-01-3,93221-02-4,99630-88-3,109215-53-4,115792-70-6,115792-73-9,139894-92-1,139973-25-4,144071-49-8,147648-81-5
D-Mannose pentaacetate

: 74761-78-7
2,3,4,6-tetra-O-acetyl-N--β-D-mannopyranosylamine

Guidance literature:: Multi-step reaction with 3 steps

1: stannic tetrachloride / CH₂Cl₂ / 6 h

2: 61 percent / H₂ / Raney nickel / ethyl acetate / 6.5 h

3: 64 percent / dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / 16 h

With hydrogen; tin(IV) chloride; dicyclohexyl-carbodiimide; nickel; In dichloromethane; ethyl acetate;
DOI:10.1016/S0008-6215(00)85529-9

Reference yield:

: 53784-29-5
2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl azide

: 74761-78-7
2,3,4,6-tetra-O-acetyl-N--β-D-mannopyranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / H₂ / Raney nickel / ethyl acetate / 6.5 h

2: 64 percent / dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / 16 h

With hydrogen; dicyclohexyl-carbodiimide; nickel; In dichloromethane; ethyl acetate;
DOI:10.1016/S0008-6215(00)85529-9