Cilobradine

Base Information

• Chemical Name: Cilobradine
• CAS No.: 109859-50-9
• Molecular Formula: C28H38 N2 O5
• Molecular Weight: 482.617
• Mol file: 109859-50-9.mol

Synonyms:Cilobradine

Chemical Property of Cilobradine

Chemical Property:

• PSA: 60.47000
• LogP: 3.47870

Purity/Quality:

Cilobradine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cilobradine

There total 2 articles about Cilobradine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

3-[(N-(2-(3,4-dimethoxy-phenyl)-ethyl)-piperidin-3-yl)methyl]-7,8-dimethoxy-1,3-dihydro-2H-3-benzazepin-2-one → 3-[(N-(2-(3,4-dimethoxy-phenyl)-ethyl)-piperidin-3-yl)-methyl]-7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one (109859-50-9)

Guidance literature:

Reference yield:

→ 3-[(N-(2-(3,4-dimethoxy-phenyl)-ethyl)-piperidin-3-yl)-methyl]-7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one (109859-50-9)

Guidance literature:

Reference yield:

3-[(N-(2-(3,4-dimethoxy-phenyl)-ethyl)-piperidin-3-yl)-methyl]-7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one (109859-50-9) → 3-[(N-(2-(3,4-Dimethoxy-phenyl)-ethyl)-piperidin-3-yl)methyl]-7,8-dimethoxy-1,3,4, 5-tetrahydro-2H-3-benzazepin-2thione-hydrochloride (109859-55-4)

Guidance literature:

With diphosphorus pentasulfide; In pyridine;

Downstream raw materials:

3-[(N-(2-(3,4-Dimethoxy-phenyl)-ethyl)-piperidin-3-yl)methyl]-7,8-dimethoxy-1,3,4, 5-tetrahydro-2H-3-benzazepin-2thione-hydrochloride

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