C₁₆H₁₅ClN₄O₃

Base Information

Chemical Name:C₁₆H₁₅ClN₄O₃
CAS No.:1412452-83-5
Molecular Formula:C₁₆H₁₅ClN₄O₃
Molecular Weight:346.773
Hs Code.:

C<sub>16</sub>H<sub>15</sub>ClN<sub>4</sub>O<sub>3</sub>

Synonyms:C₁₆H₁₅ClN₄O₃

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Chemical Property of C₁₆H₁₅ClN₄O₃

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Technology Process of C₁₆H₁₅ClN₄O₃

There total 6 articles about C₁₆H₁₅ClN₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1350300-89-8
C₁₈H₁₈ClN₃O₄

: 1412452-83-5
C₁₆H₁₅ClN₄O₃

Guidance literature:: With ammonia; In methanol; at 50 ℃; for 2h; Inert atmosphere; Microwave irradiation;
DOI:10.1021/ml300277t

Reference yield:

: 79099-07-3
N-tert-butyloxycarbonylpiperidin-4-one

: 1412452-83-5
C₁₆H₁₅ClN₄O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere; Large scale

1.2: -78 - 20 °C / Inert atmosphere; Large scale

2.1: acetic acid / 18 h / 50 °C / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 18 h / 20 °C / Inert atmosphere

3.2: 18 h / 20 °C / Inert atmosphere

4.1: trichlorophosphate / 2 h / Inert atmosphere; Reflux

5.1: ammonia / methanol / 2 h / 50 °C / Inert atmosphere; Microwave irradiation

With ammonia; acetic acid; trifluoroacetic acid; lithium hexamethyldisilazane; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ml300277t

Reference yield:

: 1412452-82-4
C₁₅H₂₁N₃O₅

: 1412452-83-5
C₁₆H₁₅ClN₄O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / dichloromethane / 18 h / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C / Inert atmosphere

2.1: trichlorophosphate / 2 h / Inert atmosphere; Reflux

3.1: ammonia / methanol / 2 h / 50 °C / Inert atmosphere; Microwave irradiation

With ammonia; trifluoroacetic acid; trichlorophosphate; In methanol; dichloromethane;
DOI:10.1021/ml300277t