(1R,9R)-10,10-Dimethyl-3,5-diphenyl-3,5-diaza-tricyclo[7.1.1.0^2,7]undec-2⁽⁷⁾-ene-4,6-dithione

Base Information

• Chemical Name: (1R,9R)-10,10-Dimethyl-3,5-diphenyl-3,5-diaza-tricyclo[7.1.1.0^2,7]undec-2⁽⁷⁾-ene-4,6-dithione
• CAS No.: 80254-34-8
• Molecular Formula: C₂₃H₂₂N₂S₂
• Molecular Weight: 390.573

Synonyms:(1R,9R)-10,10-Dimethyl-3,5-diphenyl-3,5-diaza-tricyclo[7.1.1.0^2,7]undec-2⁽⁷⁾-ene-4,6-dithione

Chemical Property of (1R,9R)-10,10-Dimethyl-3,5-diphenyl-3,5-diaza-tricyclo[7.1.1.0^2,7]undec-2⁽⁷⁾-ene-4,6-dithione

Chemical Property:

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Technology Process of (1R,9R)-10,10-Dimethyl-3,5-diphenyl-3,5-diaza-tricyclo[7.1.1.0^2,7]undec-2⁽⁷⁾-ene-4,6-dithione

There total 1 articles about (1R,9R)-10,10-Dimethyl-3,5-diphenyl-3,5-diaza-tricyclo[7.1.1.0^2,7]undec-2⁽⁷⁾-ene-4,6-dithione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1R,5S)-(+)-nopinone (38651-65-9) + phenyl isothiocyanate (103-72-0) → (1R,9R)-10,10-Dimethyl-3,5-diphenyl-3,5-diaza-tricyclo[7.1.1.02,7]undec-2(7)-ene-4,6-dithione (80254-34-8)

Guidance literature:

With sodium amide; Yield given. Multistep reaction; 1.) toluene, 4 h, reflux, 2.) toluene, 2 h at 0 deg C, then standing for 12 h;

DOI:10.1016/S0040-4020(01)88901-8

Reference yield:

(1R,9R)-10,10-Dimethyl-3,5-diphenyl-3,5-diaza-tricyclo[7.1.1.02,7]undec-2(7)-ene-4,6-dithione (80254-34-8) → (1R,9R)-10,10-Dimethyl-3,5-diphenyl-3,5-diaza-tricyclo[7.1.1.02,7]undec-2(7)-ene-4,6-dione (80254-49-5)

Guidance literature:

With mercury(II) diacetate; acetic acid; In acetone; for 48h; Yield given; Heating;

DOI:10.1016/S0040-4020(01)88901-8

upstream raw materials:

(1R,5S)-(+)-nopinone

phenyl isothiocyanate

Downstream raw materials:

(1R,9R)-10,10-Dimethyl-3,5-diphenyl-3,5-diaza-tricyclo[7.1.1.0^2,7]undec-2⁽⁷⁾-ene-4,6-dione

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