trans-ethyl 4-[4-[(hydrazinecarbonylformyl)amino]-3-nitro-phenoxy]cyclohexane-1-carboxylate

Base Information

Chemical Name:trans-ethyl 4-[4-[(hydrazinecarbonylformyl)amino]-3-nitro-phenoxy]cyclohexane-1-carboxylate
CAS No.:959939-22-1
Molecular Formula:C₁₇H₂₂N₄O₇
Molecular Weight:394.384
Hs Code.:

Synonyms:trans-ethyl 4-[4-[(hydrazinecarbonylformyl)amino]-3-nitro-phenoxy]cyclohexane-1-carboxylate

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Chemical Property of trans-ethyl 4-[4-[(hydrazinecarbonylformyl)amino]-3-nitro-phenoxy]cyclohexane-1-carboxylate

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Technology Process of trans-ethyl 4-[4-[(hydrazinecarbonylformyl)amino]-3-nitro-phenoxy]cyclohexane-1-carboxylate

There total 3 articles about trans-ethyl 4-[4-[(hydrazinecarbonylformyl)amino]-3-nitro-phenoxy]cyclohexane-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 959939-21-0
trans-ethyl 4-[4-[(methoxycarbonylformyl)amino]-3-nitro-phenoxy]cyclohexane-1-carboxylate

: 959939-22-1
trans-ethyl 4-[4-[(hydrazinecarbonylformyl)amino]-3-nitro-phenoxy]cyclohexane-1-carboxylate

Guidance literature:: With hydrazine; In ethanol; at 20 ℃; for 1h;

Reference yield:

: 959939-14-1
ethyl 4-(4-amino-3-nitro-phenoxy)cyclohexane-1-carboxylate

: 959939-22-1
trans-ethyl 4-[4-[(hydrazinecarbonylformyl)amino]-3-nitro-phenoxy]cyclohexane-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 0.5 h / 20 °C

2: hydrazine / ethanol / 1 h / 20 °C

With pyridine; hydrazine; In ethanol; dichloromethane;

Reference yield:

: 3618-04-0,75877-66-6,17159-80-7
4-hydroxycyclohexyl carboxylic acid ethyl ester

: 959939-22-1
trans-ethyl 4-[4-[(hydrazinecarbonylformyl)amino]-3-nitro-phenoxy]cyclohexane-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 16 h / 20 °C

2: pyridine / dichloromethane / 0.5 h / 20 °C

3: hydrazine / ethanol / 1 h / 20 °C

With pyridine; di-isopropyl azodicarboxylate; triphenylphosphine; hydrazine; In tetrahydrofuran; ethanol; dichloromethane;