methyl [(2R,4S,5S,S_S)-4-benzyl-2,5-diphenyl-1-(p-tolylsulfinyl)-1,3-imidazolidin-4-yl]carboxylate

Base Information

• Chemical Name: methyl [(2R,4S,5S,S_S)-4-benzyl-2,5-diphenyl-1-(p-tolylsulfinyl)-1,3-imidazolidin-4-yl]carboxylate
• CAS No.: 188760-07-8
• Molecular Formula: C₃₁H₃₀N₂O₃S
• Molecular Weight: 510.657

Synonyms:methyl [(2R,4S,5S,S_S)-4-benzyl-2,5-diphenyl-1-(p-tolylsulfinyl)-1,3-imidazolidin-4-yl]carboxylate

Chemical Property of methyl [(2R,4S,5S,S_S)-4-benzyl-2,5-diphenyl-1-(p-tolylsulfinyl)-1,3-imidazolidin-4-yl]carboxylate

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Technology Process of methyl [(2R,4S,5S,S_S)-4-benzyl-2,5-diphenyl-1-(p-tolylsulfinyl)-1,3-imidazolidin-4-yl]carboxylate

There total 5 articles about methyl [(2R,4S,5S,S_S)-4-benzyl-2,5-diphenyl-1-(p-tolylsulfinyl)-1,3-imidazolidin-4-yl]carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

(E)-2-(benzylidene-amino)-3-phenyl-propionic acid methyl ester (339190-42-0) + (S,E)-N-benzylidene-4-methylbenzenesulfinamide (350479-90-2) → methyl [(2R,4S,5S,SS)-4-benzyl-2,5-diphenyl-1-(p-tolylsulfinyl)-1,3-imidazolidin-4-yl]carboxylate (188760-07-8) + (-)-methyl [(2S,4R,5R,SS)-4-benzyl-2,5-diphenyl-1-(p-tolylsulfinyl)-1,3-imidazolidin-4-yl]carboxylate (188760-06-7)

Guidance literature:

(E)-2-(benzylidene-amino)-3-phenyl-propionic acid methyl ester; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.416667h;

(S,E)-N-benzylidene-4-methylbenzenesulfinamide; In tetrahydrofuran; at -78 - 4 ℃; for 20h; Further stages.;

DOI:10.1002/chem.200204674

Reference yield: 36.0%

(E)-2-(benzylidene-amino)-3-phenyl-propionic acid methyl ester (339190-42-0) + (S,E)-N-benzylidene-4-methylbenzenesulfinamide (350479-90-2) → methyl [(2R,4S,5S,SS)-4-benzyl-2,5-diphenyl-1-(p-tolylsulfinyl)-1,3-imidazolidin-4-yl]carboxylate (188760-07-8) + (2S,4S,5R)-4-Benzyl-2,5-diphenyl-1-p-tolylsulfanyl-imidazolidine-4-carboxylic acid methyl ester + methyl [(2R,4R,5S,SS)-4-benzyl-2,5-diphenyl-1-(p-tolylsulfinyl)-1,3-imidazolidin-4-yl]carboxylate + (-)-methyl [(2S,4S,5R,SS)-4-benzyl-2,5-diphenyl-1-(p-tolylsulfinyl)-1,3-imidazolidin-4-yl]carboxylate (596823-56-2)

Guidance literature:

(E)-2-(benzylidene-amino)-3-phenyl-propionic acid methyl ester; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃;

(S,E)-N-benzylidene-4-methylbenzenesulfinamide; With titanium tetrachloride; In tetrahydrofuran; at -78 - -20 ℃;

In chloroform; at 20 ℃; Further stages.;

DOI:10.1002/chem.200204674

Reference yield: 25.0%

(E)-2-(benzylidene-amino)-3-phenyl-propionic acid methyl ester (339190-42-0) + (S,E)-N-benzylidene-4-methylbenzenesulfinamide (350479-90-2) → methyl [(2R,4S,5S,SS)-4-benzyl-2,5-diphenyl-1-(p-tolylsulfinyl)-1,3-imidazolidin-4-yl]carboxylate (188760-07-8) + methyl [(2R,4R,5S,SS)-4-benzyl-2,5-diphenyl-1-(p-tolylsulfinyl)-1,3-imidazolidin-4-yl]carboxylate + (-)-methyl [(2S,4S,5R,SS)-4-benzyl-2,5-diphenyl-1-(p-tolylsulfinyl)-1,3-imidazolidin-4-yl]carboxylate (596823-56-2)

Guidance literature:

(E)-2-(benzylidene-amino)-3-phenyl-propionic acid methyl ester; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃;

(S,E)-N-benzylidene-4-methylbenzenesulfinamide; With bis(cyclopentadienyl)titanium dichloride; In tetrahydrofuran; at -78 - -20 ℃;

In chloroform; at 20 ℃; Further stages.;

DOI:10.1002/chem.200204674

upstream raw materials:

(S,E)-N-benzylidene-4-methylbenzenesulfinamide

(E)-2-(benzylidene-amino)-3-phenyl-propionic acid methyl ester

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