diphenylboryl 5,5,5-trichloro-4-aminopent-3-en-2-one

Base Information

Chemical Name:diphenylboryl 5,5,5-trichloro-4-aminopent-3-en-2-one
CAS No.:151627-74-6
Molecular Formula:C₁₇H₁₅BCl₃NO
Molecular Weight:366.482
Hs Code.:

Synonyms:diphenylboryl 5,5,5-trichloro-4-aminopent-3-en-2-one

Suppliers and Price of diphenylboryl 5,5,5-trichloro-4-aminopent-3-en-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of diphenylboryl 5,5,5-trichloro-4-aminopent-3-en-2-one

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of diphenylboryl 5,5,5-trichloro-4-aminopent-3-en-2-one

There total 4 articles about diphenylboryl 5,5,5-trichloro-4-aminopent-3-en-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.5%

: 37147-02-7
5,5,5-trichloro-4-amino-3-penten-2-one

: 15323-04-3
diphenylborinic acid butyl ester

: 151627-74-6
diphenylboryl 5,5,5-trichloro-4-aminopent-3-en-2-one

Guidance literature:: In diethyl ether; byproducts: butanol; stirred for 1 h; allowed to stand for 12 h; reaction of equilibrium;; evapd. (2 mmHg, 50.60°C); pantane added; ppt. filtered; washed with pentane;;
DOI:10.1007/BF00863380

Reference yield: 92.0%

: 37147-02-7
5,5,5-trichloro-4-amino-3-penten-2-one

: 61209-21-0
(butylthio)diphenylborane

: 151627-74-6
diphenylboryl 5,5,5-trichloro-4-aminopent-3-en-2-one

Guidance literature:: In diethyl ether; byproducts: BuSH; stirred for 15 min; allowed to stand for 12 h;; evapd.; pantane added; ppt. filtered; washed with pentane; elem. anal.;;
DOI:10.1007/BF00863380