C₂₃H₂₂O

Base Information

Chemical Name:C₂₃H₂₂O
CAS No.:1591812-60-0
Molecular Formula:C₂₃H₂₂O
Molecular Weight:314.427
Hs Code.:

Synonyms:C₂₃H₂₂O

Suppliers and Price of C₂₃H₂₂O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₂₂O

Chemical Property:

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Technology Process of C₂₃H₂₂O

There total 3 articles about C₂₃H₂₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1591812-47-3
C₂₃H₂₄O₂

: 1591812-60-0
C₂₃H₂₂O

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/ejoc.201301537

Reference yield:

: 1591812-50-8
C₁₂H₁₀O

: 1591812-60-0
C₂₃H₂₂O

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(I) bromide dimethylsulfide complex / tetrahydrofuran; dibutyl ether / 0.75 h / 0 °C / Inert atmosphere

1.2: 0.5 h / -78 °C / Inert atmosphere

2.1: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

With copper(I) bromide dimethylsulfide complex; boron trifluoride diethyl etherate; In tetrahydrofuran; dichloromethane; dibutyl ether;
DOI:10.1002/ejoc.201301537

Reference yield:

: 141868-93-1,141868-92-0
(E)-N-methoxy-N-methyl-3-phenylbut-2-enamide

: 1591812-60-0
C₂₃H₂₂O

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 0 °C / Inert atmosphere

2.1: copper(I) bromide dimethylsulfide complex / tetrahydrofuran; dibutyl ether / 0.75 h / 0 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

3.1: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

With copper(I) bromide dimethylsulfide complex; boron trifluoride diethyl etherate; In tetrahydrofuran; dichloromethane; dibutyl ether;
DOI:10.1002/ejoc.201301537