2-acetamido-7-<4-(tert-butoxycarbonyl)phenyl>-5-deaza-6,7,8,9-tetrahydro-4(3H)-pyrido<3,4-g>pteridinone

Base Information

Chemical Name:2-acetamido-7-<4-(tert-butoxycarbonyl)phenyl>-5-deaza-6,7,8,9-tetrahydro-4(3H)-pyrido<3,4-g>pteridinone
CAS No.:95017-86-0
Molecular Formula:C₂₃H₂₅N₅O₄
Molecular Weight:435.483
Hs Code.:

Synonyms:2-acetamido-7-<4-(tert-butoxycarbonyl)phenyl>-5-deaza-6,7,8,9-tetrahydro-4(3H)-pyrido<3,4-g>pteridinone

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Chemical Property of 2-acetamido-7-<4-(tert-butoxycarbonyl)phenyl>-5-deaza-6,7,8,9-tetrahydro-4(3H)-pyrido<3,4-g>pteridinone

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Technology Process of 2-acetamido-7-<4-(tert-butoxycarbonyl)phenyl>-5-deaza-6,7,8,9-tetrahydro-4(3H)-pyrido<3,4-g>pteridinone

There total 6 articles about 2-acetamido-7-<4-(tert-butoxycarbonyl)phenyl>-5-deaza-6,7,8,9-tetrahydro-4(3H)-pyrido<3,4-g>pteridinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 108-24-7
acetic anhydride

: 95017-85-9
2-amino-7-<4-(tert-butoxycarbonyl)phenyl>-5-deaza-6,7,8,9-tetrahydro-4(3H)-pyrido<3,4-g>pteridinone

: 95017-86-0
2-acetamido-7-<4-(tert-butoxycarbonyl)phenyl>-5-deaza-6,7,8,9-tetrahydro-4(3H)-pyrido<3,4-g>pteridinone

Guidance literature:: With dmap; for 1h; Heating;
DOI:10.1021/jo00207a020

Reference yield:

: 5382-16-1
4-HYDROXYPIPERIDINE

: 95017-86-0
2-acetamido-7-<4-(tert-butoxycarbonyl)phenyl>-5-deaza-6,7,8,9-tetrahydro-4(3H)-pyrido<3,4-g>pteridinone

Guidance literature:: Multi-step reaction with 5 steps

1: 73 percent / K₂CO₃ / dimethylsulfoxide / 7 h / 120 °C

2: 83 percent / dicyclohexylcarbodiimide, pyridine, trifluoroacetic acid / dimethylsulfoxide; benzene / 5 °C

4: 51 percent / piperidine / acetic acid; H₂O / 2 h / Heating

5: 76 percent / 4-(dimethylamino)pyridine / 1 h / Heating

With piperidine; pyridine; dmap; potassium carbonate; dicyclohexyl-carbodiimide; trifluoroacetic acid; In water; acetic acid; dimethyl sulfoxide; benzene;
DOI:10.1021/jo00207a020

Reference yield:

: 58656-98-7
tert-butyl 4-fluorobenzoate

: 95017-86-0
2-acetamido-7-<4-(tert-butoxycarbonyl)phenyl>-5-deaza-6,7,8,9-tetrahydro-4(3H)-pyrido<3,4-g>pteridinone

Guidance literature:: Multi-step reaction with 5 steps

1: 73 percent / K₂CO₃ / dimethylsulfoxide / 7 h / 120 °C

2: 83 percent / dicyclohexylcarbodiimide, pyridine, trifluoroacetic acid / dimethylsulfoxide; benzene / 5 °C

4: 51 percent / piperidine / acetic acid; H₂O / 2 h / Heating

5: 76 percent / 4-(dimethylamino)pyridine / 1 h / Heating

With piperidine; pyridine; dmap; potassium carbonate; dicyclohexyl-carbodiimide; trifluoroacetic acid; In water; acetic acid; dimethyl sulfoxide; benzene;
DOI:10.1021/jo00207a020