6-methyl-1-(phenylsulfonyl)-3,4,5,6-tetrahydro-1H-azepino[5,4,3-cd]indol-7-yl trifluoromethanesulfonate trifluoroacetate

Base Information

Chemical Name:6-methyl-1-(phenylsulfonyl)-3,4,5,6-tetrahydro-1H-azepino[5,4,3-cd]indol-7-yl trifluoromethanesulfonate trifluoroacetate
CAS No.:1059129-28-0
Molecular Formula:C₂HF₃O₂*C₁₉H₁₇F₃N₂O₅S₂
Molecular Weight:588.506
Hs Code.:

Synonyms:6-methyl-1-(phenylsulfonyl)-3,4,5,6-tetrahydro-1H-azepino[5,4,3-cd]indol-7-yl trifluoromethanesulfonate trifluoroacetate

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Chemical Property of 6-methyl-1-(phenylsulfonyl)-3,4,5,6-tetrahydro-1H-azepino[5,4,3-cd]indol-7-yl trifluoromethanesulfonate trifluoroacetate

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Technology Process of 6-methyl-1-(phenylsulfonyl)-3,4,5,6-tetrahydro-1H-azepino[5,4,3-cd]indol-7-yl trifluoromethanesulfonate trifluoroacetate

There total 5 articles about 6-methyl-1-(phenylsulfonyl)-3,4,5,6-tetrahydro-1H-azepino[5,4,3-cd]indol-7-yl trifluoromethanesulfonate trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1059131-23-5
tert-butyl 6-methyl-1-(phenylsulfonyl)-7-([(trifluoromethyl)sulfonyl]oxy)-1,3,4,6-tetrahydro-5H-azepino[5,4,3-cd]indole-5-carboxylate

: 76-05-1
trifluoroacetic acid

: 1059129-28-0
6-methyl-1-(phenylsulfonyl)-3,4,5,6-tetrahydro-1H-azepino[5,4,3-cd]indol-7-yl trifluoromethanesulfonate trifluoroacetate

Guidance literature:: In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 1059131-20-2
tert-butyl 7-(acetyloxy)-6-methyl-1,3,4,6-tetrahydro-5H-azepino[5,4,3-cd]indole-5-carboxylate

: 1059129-28-0
6-methyl-1-(phenylsulfonyl)-3,4,5,6-tetrahydro-1H-azepino[5,4,3-cd]indol-7-yl trifluoromethanesulfonate trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.05 h / 0 °C

1.2: 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

3.1: dichloromethane / 1 h / 20 °C

With sodium hydride; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1059131-22-4
tert-butyl 7-hydroxy-6-methyl-1-(phenylsulfonyl)-1,3,4,6-tetrahydro-5H-azepino[5,4,3-cd]indole-5-carboxylate

: 1059129-28-0
6-methyl-1-(phenylsulfonyl)-3,4,5,6-tetrahydro-1H-azepino[5,4,3-cd]indol-7-yl trifluoromethanesulfonate trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

2: dichloromethane / 1 h / 20 °C

With N-ethyl-N,N-diisopropylamine; In dichloromethane;