trihydrido(4-κN-[3-(2-hydroxy-ethyl)-benzyl]-piperazine-1-carboxylic acid tert-butyl ester)boron

Base Information

Chemical Name:trihydrido(4-κN-[3-(2-hydroxy-ethyl)-benzyl]-piperazine-1-carboxylic acid tert-butyl ester)boron
CAS No.:950504-60-6
Molecular Formula:C₁₈H₃₁BN₂O₃
Molecular Weight:334.267
Hs Code.:

Synonyms:trihydrido(4-κN-[3-(2-hydroxy-ethyl)-benzyl]-piperazine-1-carboxylic acid tert-butyl ester)boron

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Chemical Property of trihydrido(4-κN-[3-(2-hydroxy-ethyl)-benzyl]-piperazine-1-carboxylic acid tert-butyl ester)boron

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Technology Process of trihydrido(4-κN-[3-(2-hydroxy-ethyl)-benzyl]-piperazine-1-carboxylic acid tert-butyl ester)boron

There total 4 articles about trihydrido(4-κN-[3-(2-hydroxy-ethyl)-benzyl]-piperazine-1-carboxylic acid tert-butyl ester)boron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tert-butyl 4-[[3-(2-hydroxyethyl)phenyl]methyl]piperazine-1-carboxylate

: 950504-60-6
trihydrido(4-κN-[3-(2-hydroxy-ethyl)-benzyl]-piperazine-1-carboxylic acid tert-butyl ester)boron

Guidance literature:: With dimethylsulfide borane complex; In tetrahydrofuran; at 0 ℃; for 0.0833333h;

Reference yield:

: 142327-44-4
methyl 3-formylphenylacetate

: 950504-60-6
trihydrido(4-κN-[3-(2-hydroxy-ethyl)-benzyl]-piperazine-1-carboxylic acid tert-butyl ester)boron

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride; acetic acid / methanol / 24 h

2: sodium tetrahydroborate; calcium chloride / ethanol

3: dimethylsulfide borane complex / tetrahydrofuran / 0.08 h / 0 °C

With sodium tetrahydroborate; dimethylsulfide borane complex; sodium tris(acetoxy)borohydride; acetic acid; calcium chloride; In tetrahydrofuran; methanol; ethanol;

Reference yield:

: C₁₉H₂₈N₂O₄

: 950504-60-6
trihydrido(4-κN-[3-(2-hydroxy-ethyl)-benzyl]-piperazine-1-carboxylic acid tert-butyl ester)boron

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; calcium chloride / ethanol

2: dimethylsulfide borane complex / tetrahydrofuran / 0.08 h / 0 °C

With sodium tetrahydroborate; dimethylsulfide borane complex; calcium chloride; In tetrahydrofuran; ethanol;