BLDA

Base Information

• Chemical Name: BLDA
• CAS No.: 406728-60-7
• Molecular Formula: C₂₄H₃₉N₃O₇
• Molecular Weight: 481.59
• Mol file: 406728-60-7.mol

Synonyms:BLDA

Chemical Property of BLDA

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of BLDA

There total 5 articles about BLDA which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

→ BLDA (406728-60-7)

Guidance literature:

Reference yield: 71.0%

N,N'-di-t-butyloxycarbonyl-(S)-lysine N-hydroxysuccinimide ester (30189-36-7) + dopamine hydrochloride (62-31-7) → BLDA (406728-60-7)

Guidance literature:

With triethylamine; In methanol; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1039/c2jm16598h

Reference yield:

L-lysine (56-87-1,3506-25-0) → BLDA (406728-60-7)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / tetrahydrofuran; water / 24 h / 30 °C / Inert atmosphere

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 - 20 °C

3: triethylamine / methanol / 12 h / 20 °C / Inert atmosphere

With sodium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water;

DOI:10.1039/c2jm16598h

upstream raw materials:

N,N'-di-t-butyloxycarbonyl-(S)-lysine N-hydroxysuccinimide ester

dopamine hydrochloride

L-lysine

di-tert-butyl dicarbonate

Downstream raw materials:

LDA