molybdenum tris[1,2-bis(trifluoromethyl)ethane-1,2-dithiolene]

Base Information

• Chemical Name: molybdenum tris[1,2-bis(trifluoromethyl)ethane-1,2-dithiolene]
• CAS No.: 1494-07-1
• Molecular Formula: C₁₂F₁₈MoS₆
• Molecular Weight: 774.439

Synonyms:molybdenum tris[1,2-bis(trifluoromethyl)ethane-1,2-dithiolene]

Chemical Property of molybdenum tris[1,2-bis(trifluoromethyl)ethane-1,2-dithiolene]

Chemical Property:

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: Molybdenum tris(1,2-bis(trifluoromethyl)ethane-1,2-dithiolene) (Mo(tfd)3) may be used to p dope the hole transporting layer of HTM N,N′-di[(1-naphthyl)-N,N′-diphenyl]-1,1′-biphenyl-4,4′- diamine. It may be used as a dopant to reduced contact resistance in pentacene based organic field effect transistors (OFETs).

Technology Process of molybdenum tris[1,2-bis(trifluoromethyl)ethane-1,2-dithiolene]

There total 3 articles about molybdenum tris[1,2-bis(trifluoromethyl)ethane-1,2-dithiolene] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-bis-trifluoromethyl-[1,2]dithiete (360-91-8) + molybdenum hexacarbonyl (13939-06-5,199620-15-0) → molybdenum tris[1,2-bis(trifluoromethyl)ethane-1,2-dithiolene] (1494-07-1)

Guidance literature:

In methyl cyclohexane; reflux; 18 h;

DOI:10.1021/ic50007a056

Reference yield:

Mo(S2C2(CF3)2)2(2,5-dihydrothiophene)2 (1251146-86-7) → molybdenum tris[1,2-bis(trifluoromethyl)ethane-1,2-dithiolene] (1494-07-1)

Guidance literature:

In chloroform-d1; byproducts: thiophene; heating at 60°C for 20 or gradual heating at 60°C (24 h) and then at 120°C (5 h); detd. by (1)H NMR spectroscopy;

DOI:10.1002/ejic.201000269

Reference yield:

Mo(S2C2(CF3)2)2(tetrahydrothiophene)2 (1251146-87-8) → molybdenum tris[1,2-bis(trifluoromethyl)ethane-1,2-dithiolene] (1494-07-1)

Guidance literature:

In chloroform; decompn. in CHCl3 within few days at room temp. or within 1 h at 60°C;

DOI:10.1002/ejic.201000269

upstream raw materials:

3,4-bis-trifluoromethyl-[1,2]dithiete

molybdenum hexacarbonyl

Mo(S₂C₂(CF₃)2)2(2,5-dihydrothiophene)2

Mo(S₂C₂(CF₃)2)2(tetrahydrothiophene)2

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