8-acetoxy-13-(3-methyl-butyrylamino)-2-oxo-11-phenyl-10-oxa-6-thia-3,12-diaza-tricyclo[7.3.1.0^3,7]tridec-11-ene-4-carboxylic acid methyl ester

Base Information

• Chemical Name: 8-acetoxy-13-(3-methyl-butyrylamino)-2-oxo-11-phenyl-10-oxa-6-thia-3,12-diaza-tricyclo[7.3.1.0^3,7]tridec-11-ene-4-carboxylic acid methyl ester
• CAS No.: 872094-48-9
• Molecular Formula: C₂₄H₂₉N₃O₇S
• Molecular Weight: 503.576

Synonyms:8-acetoxy-13-(3-methyl-butyrylamino)-2-oxo-11-phenyl-10-oxa-6-thia-3,12-diaza-tricyclo[7.3.1.0^3,7]tridec-11-ene-4-carboxylic acid methyl ester

Chemical Property of 8-acetoxy-13-(3-methyl-butyrylamino)-2-oxo-11-phenyl-10-oxa-6-thia-3,12-diaza-tricyclo[7.3.1.0^3,7]tridec-11-ene-4-carboxylic acid methyl ester

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Technology Process of 8-acetoxy-13-(3-methyl-butyrylamino)-2-oxo-11-phenyl-10-oxa-6-thia-3,12-diaza-tricyclo[7.3.1.0^3,7]tridec-11-ene-4-carboxylic acid methyl ester

There total 8 articles about 8-acetoxy-13-(3-methyl-butyrylamino)-2-oxo-11-phenyl-10-oxa-6-thia-3,12-diaza-tricyclo[7.3.1.0^3,7]tridec-11-ene-4-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

8-hydroxy-13-(3-methyl-butyrylamino)-2-oxo-11-phenyl-10-oxa-6-thia-3,12-diaza-tricyclo[7.3.1.03,7]tridec-11-ene-4-carboxylic acid methyl ester (872094-47-8) + acetic anhydride (108-24-7) → 8-acetoxy-13-(3-methyl-butyrylamino)-2-oxo-11-phenyl-10-oxa-6-thia-3,12-diaza-tricyclo[7.3.1.03,7]tridec-11-ene-4-carboxylic acid methyl ester (872094-48-9)

Guidance literature:

With pyridine; at 40 ℃; for 48h;

DOI:10.1002/chem.200500515

Reference yield:

2-amino-3-azido-4-oxo-octahydro-1-oxa-7-thia-4a-aza-cyclopropa[e]azulene-5-carboxylic acid methyl ester (872094-45-6) → 8-acetoxy-13-(3-methyl-butyrylamino)-2-oxo-11-phenyl-10-oxa-6-thia-3,12-diaza-tricyclo[7.3.1.03,7]tridec-11-ene-4-carboxylic acid methyl ester (872094-48-9)

Guidance literature:

Multi-step reaction with 4 steps

1: 87 percent / pyridine / dimethylformamide / 0.33 h / 20 °C

2: H₂ / Pd/C / methanol / 3 h

3: 480 mg / pyridine / 0.5 h

4: 100 percent / pyridine / 48 h / 40 °C

With pyridine; hydrogen; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;

DOI:10.1002/chem.200500515

Reference yield:

3-azido-2-(3-methyl-butyrylamino)-4-oxo-octahydro-1-oxa-7-thia-4a-aza-cyclopropa[e]azulene-5-carboxylic acid methyl ester (872094-46-7) → 8-acetoxy-13-(3-methyl-butyrylamino)-2-oxo-11-phenyl-10-oxa-6-thia-3,12-diaza-tricyclo[7.3.1.03,7]tridec-11-ene-4-carboxylic acid methyl ester (872094-48-9)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂ / Pd/C / methanol / 3 h

2: 480 mg / pyridine / 0.5 h

3: 100 percent / pyridine / 48 h / 40 °C

With pyridine; hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1002/chem.200500515

upstream raw materials:

8-hydroxy-13-(3-methyl-butyrylamino)-2-oxo-11-phenyl-10-oxa-6-thia-3,12-diaza-tricyclo[7.3.1.0^3,7]tridec-11-ene-4-carboxylic acid methyl ester

acetic anhydride

2-amino-3-azido-4-oxo-octahydro-1-oxa-7-thia-4a-aza-cyclopropa[e]azulene-5-carboxylic acid methyl ester

4-oxo-3-trifluoromethanesulfonyloxy-1a,4,5,6,7a,7b-hexahydro-1-oxa-7-thia-4a-aza-cyclopropa[e]azulene-5-carboxylic acid methyl ester

Downstream raw materials:

9-acetoxy-6-benzoylamino-8-hydroxy-7-(3-methyl-butyrylamino)-5-oxo-octahydro-thiazolo[3,2-a]azepine-3-carboxylic acid methyl ester

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