(S)-N-[3,5-bis(benzyloxy)phenethyl]-2-(dibenzylamino)-5-hydroxypentanamide

Base Information

Chemical Name:(S)-N-[3,5-bis(benzyloxy)phenethyl]-2-(dibenzylamino)-5-hydroxypentanamide
CAS No.:1327254-70-5
Molecular Formula:C₄₁H₄₄N₂O₄
Molecular Weight:628.811
Hs Code.:

Synonyms:(S)-N-[3,5-bis(benzyloxy)phenethyl]-2-(dibenzylamino)-5-hydroxypentanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-[3,5-bis(benzyloxy)phenethyl]-2-(dibenzylamino)-5-hydroxypentanamide

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Technology Process of (S)-N-[3,5-bis(benzyloxy)phenethyl]-2-(dibenzylamino)-5-hydroxypentanamide

There total 1 articles about (S)-N-[3,5-bis(benzyloxy)phenethyl]-2-(dibenzylamino)-5-hydroxypentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 850209-98-2
(S)-2-dibenzylamino-5-hydroxypentanoic acid benzyl ester

: 188662-05-7
<2-<3,5-bis(benzyloxy)phenyl>ethyl>amine

: 1327254-70-5
(S)-N-[3,5-bis(benzyloxy)phenethyl]-2-(dibenzylamino)-5-hydroxypentanamide

Guidance literature:: <2-<3,5-bis(benzyloxy)phenyl>ethyl>amine; With diisobutylaluminium hydride; In tetrahydrofuran; hexane; at 0 - 20 ℃; Inert atmosphere;

(S)-2-dibenzylamino-5-hydroxypentanoic acid benzyl ester; In tetrahydrofuran; hexane; for 17h; Reflux; Inert atmosphere;
DOI:10.1016/j.tet.2011.06.023

Reference yield: 91.0%

: 1327254-70-5
(S)-N-[3,5-bis(benzyloxy)phenethyl]-2-(dibenzylamino)-5-hydroxypentanamide

: 1327254-59-0
(3S)-1-[3,5-bis(benzyloxy)phenethyl]-3-(dibenzylamino)-6-hydroxypiperidin-2-one

Guidance literature:: (S)-N-[3,5-bis(benzyloxy)phenethyl]-2-(dibenzylamino)-5-hydroxypentanamide; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.666667h;

With triethylamine; In dichloromethane; at -78 - 5 ℃; for 0.5h; optical yield given as %de;
DOI:10.1016/j.tet.2011.06.023