C₃₉H₄₆O₁₂

Base Information

Chemical Name:C₃₉H₄₆O₁₂
CAS No.:153145-53-0
Molecular Formula:C₃₉H₄₆O₁₂
Molecular Weight:706.787
Hs Code.:

C<sub>39</sub>H<sub>46</sub>O<sub>12</sub>

Synonyms:C₃₉H₄₆O₁₂

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Chemical Property of C₃₉H₄₆O₁₂

Chemical Property:

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Technology Process of C₃₉H₄₆O₁₂

There total 51 articles about C₃₉H₄₆O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 153145-52-9
C₄₅H₆₀O₁₂Si

: 153145-53-0
C₃₉H₄₆O₁₂

Guidance literature:: With tris(dimethylamino)sulfonium trimethylsilyldifluoride; In tetrahydrofuran; at 25 ℃; for 1h;

Reference yield:

: 153145-26-7
C₃₂H₅₆O₇Si₂

: 153145-53-0
C₃₉H₄₆O₁₂

Guidance literature:: Multi-step reaction with 14 steps

1: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

2: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

3: 95 percent / CH₂Cl₂ / 15 h / -45 °C

4: 63 percent / Burgess' reagent

5: 100 percent / pyridine

6: 65 percent / OsO₄

7: DBU / toluene / 2 h / 105 °C

8: 75 percent / pyridine, DMAP / 24 h / 25 °C

9: 100 percent / HF*pyridine / acetonitrile / 11 h / 0 °C

10: tetrahydrofuran / 0.17 h / -78 °C

11: tetrapropylammonium perruthenate, NMO, molecular sieves / CH₂Cl₂ / 0.25 h / 25 °C

12: 1.) t-BuOK, 2.) benzeneseleninic anhydride, 3.) t-BuOK

13: pyridine, DMAP / 20 h / 25 °C

14: 94 percent / TASF / tetrahydrofuran / 1 h / 25 °C

With pyridine; dmap; osmium(VIII) oxide; N-methyl-2-indolinone; molecular sieve; tetrapropylammonium perruthennate; Burgess Reagent; benzeneseleninic anhydride; potassium tert-butylate; tris(dimethylamino)sulfonium trimethylsilyldifluoride; tetra-(n-butyl)ammonium iodide; pyridine hydrogenfluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; toluene; acetonitrile;

Reference yield:

: 153145-20-1
C₃₄H₅₈O₇Si₂

: 153145-53-0
C₃₉H₄₆O₁₂

Guidance literature:: Multi-step reaction with 21 steps

1: O₃

2: KMnO₄, KH₂PO₄

4: 93 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

5: 100 percent / p-TsOH

6: 92 percent / PhSK / dimethylformamide / 3 h / 86 °C

7: acid

8: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

9: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

10: 95 percent / CH₂Cl₂ / 15 h / -45 °C

11: 63 percent / Burgess' reagent

12: 100 percent / pyridine

13: 65 percent / OsO₄

14: DBU / toluene / 2 h / 105 °C

15: 75 percent / pyridine, DMAP / 24 h / 25 °C

16: 100 percent / HF*pyridine / acetonitrile / 11 h / 0 °C

17: tetrahydrofuran / 0.17 h / -78 °C

18: tetrapropylammonium perruthenate, NMO, molecular sieves / CH₂Cl₂ / 0.25 h / 25 °C

19: 1.) t-BuOK, 2.) benzeneseleninic anhydride, 3.) t-BuOK

20: pyridine, DMAP / 20 h / 25 °C

21: 94 percent / TASF / tetrahydrofuran / 1 h / 25 °C

With pyridine; dmap; potassium permanganate; potassium dihydrogenphosphate; osmium(VIII) oxide; N-methyl-2-indolinone; molecular sieve; tetrapropylammonium perruthennate; Burgess Reagent; benzeneseleninic anhydride; potassium tert-butylate; tris(dimethylamino)sulfonium trimethylsilyldifluoride; tetra-(n-butyl)ammonium iodide; (2E)-3-(4-hydroxyphenyl-3-methoxyphenyl)-1-phenylprop-2-en-1-one; toluene-4-sulfonic acid; pyridine hydrogenfluoride; ozone; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;