Pt(((C₆H₅)2P)2CH₂)(CCCH₃)2

Base Information

• Chemical Name: Pt(((C₆H₅)2P)2CH₂)(CCCH₃)2
• CAS No.: 88690-36-2
• Molecular Formula: C₃₁H₂₈P₂Pt
• Molecular Weight: 657.591
• Mol file: 88690-36-2.mol

Synonyms:Pt(((C₆H₅)2P)2CH₂)(CCCH₃)2

Chemical Property of Pt(((C₆H₅)2P)2CH₂)(CCCH₃)2

Chemical Property:

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Technology Process of Pt(((C₆H₅)2P)2CH₂)(CCCH₃)2

There total 1 articles about Pt(((C₆H₅)2P)2CH₂)(CCCH₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

PtCl2(dppm) (52595-94-5) + prop-1-yne (74-99-7) → Pt(((C6H5)2P)2CH2)(CCCH3)2 (88690-36-2)

Guidance literature:

With sodium methylate; In methanol; byproducts: CH3OH, NaCl; MeCCH bubbled through a suspn. of the complex in MeOH, soln. of NaOMe added slowly (over a period of 1 h), stirred for further 2 h; MeOH removed in vacuo, dissolved in benzene, filtered, addn. of pentanegave crystals, further yield obtained by freeze drying the benzene soln., elem. anal.;

DOI:10.1021/om00122a009

upstream raw materials:

PtCl₂(dppm)

prop-1-yne