[Pt(o-C₆H₄O₂)(PPh₂CCCPh)2]

Base Information

Chemical Name:[Pt(o-C₆H₄O₂)(PPh₂CCCPh)2]
CAS No.:151305-83-8
Molecular Formula:C₄₆H₃₄O₂P₂Pt
Molecular Weight:875.802
Hs Code.:

[Pt(o-C<sub>6</sub>H<sub>4</sub>O<sub>2</sub>)(PPh<sub>2</sub>CCCPh)2]

Synonyms:[Pt(o-C₆H₄O₂)(PPh₂CCCPh)2]

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Chemical Property of [Pt(o-C₆H₄O₂)(PPh₂CCCPh)2]

Chemical Property:

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Technology Process of [Pt(o-C₆H₄O₂)(PPh₂CCCPh)2]

There total 4 articles about [Pt(o-C₆H₄O₂)(PPh₂CCCPh)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 42847-16-5,30173-84-3
cis-dichlorobis(diphenyl(phenylethynyl)phosphine)platinum(II)

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 151305-83-8
[Pt(o-C₆H₄O₂)(PPh₂CCCPh)2]

Guidance literature:: With NaOH; In methanol; chloroform; treating a soln. of Pt-complex in chloroform with a soln. of catechol and NaOH in methanol at ambient temperature, refluxing for 1 h; removing ppt., evapn. of filtrate, dissolving in chloroform, washing (water), drying (Na2SO4), removing solvent, chromy. (Et2O), evapn. of eluate, washing (Et2O), recrystn. (petroleum ether-chloroform), elem. anal.;

Reference yield: 66.0%

: 7608-17-5
2-diphenylphosphino-1-phenylethyne

: 819851-69-9
[Pt(o-C₆H₄O₂)(dimethyl sulfoxide)2]

: 151305-83-8
[Pt(o-C₆H₄O₂)(PPh₂CCCPh)2]

Guidance literature:: In dichloromethane; under N2; a suspn. of Pt-contg. compd. (0.436 mmol) in CH2Cl2 was treated with PPh2CCPh (0.915 mmol); stirring for 2 h; the soln. was filtered and evapd. to dryness; the rsidue was treated with a mixt. of 1:1 Et2O/n-hexane; recrystn. from CH2Cl2/diethyl ether;
DOI:10.1021/ic048987j

Reference yield:

: 5633-97-6,50585-47-2,93692-31-0
potassium pyrocatecholate

: 151305-83-8
[Pt(o-C₆H₄O₂)(PPh₂CCCPh)2]

Guidance literature:: Multi-step reaction with 2 steps

1: methanol

2: dichloromethane

In methanol; dichloromethane;
DOI:10.1021/ic048987j