C₁₄H₁₇ClO₃

Base Information

Chemical Name:C₁₄H₁₇ClO₃
CAS No.:1027659-22-8
Molecular Formula:C₁₄H₁₇ClO₃
Molecular Weight:268.74
Hs Code.:

C<sub>14</sub>H<sub>17</sub>ClO<sub>3</sub>

Synonyms:C₁₄H₁₇ClO₃

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Chemical Property of C₁₄H₁₇ClO₃

Chemical Property:

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Technology Process of C₁₄H₁₇ClO₃

There total 1 articles about C₁₄H₁₇ClO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1615-02-7,940-62-5
3-(4-chlorophenyl)prop-2-enoic acid

: 1027659-22-8
C₁₄H₁₇ClO₃

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / H₂ / 10percent Pd-C / tetrahydrofuran / 4 h / Ambient temperature

2: Et₃N / tetrahydrofuran / 1.) -78 deg C, 15 min, 2.) 0 deg C, 45 min

With hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1021/jo00088a009

Reference yield:

: 1027659-22-8
C₁₄H₁₇ClO₃

: 57292-44-1
N-Boc-D-(4-Cl)Phe-OH

Guidance literature:: Multi-step reaction with 4 steps

1: 1) n-BuLi / 1) hexane, THF, -78 deg C, 2) a) -78 deg C, 15 min, b) up to room temp., 45 min

2: 1) KHMDS, 2) trisyl azide / 1) THF, -78 deg C, 30 min, 2) THF, -78 deg C, 2 min

3: aq. LiOH, 30percent H₂O₂ / tetrahydrofuran; H₂O / 1 h / 0 °C

4: H₂ / 10percent Pd/C / ethyl acetate / 760 Torr / Ambient temperature

With lithium hydroxide; n-butyllithium; 2,4,6-Triisopropylbenzenesulfonyl azide; hydrogen; dihydrogen peroxide; potassium hexamethylsilazane; palladium on activated charcoal; In tetrahydrofuran; water; ethyl acetate;
DOI:10.1021/jo00032a028

Reference yield:

: 1027659-22-8
C₁₄H₁₇ClO₃

: 51301-86-1,57292-44-1,129101-26-4,68090-88-0
Boc-p-chloro-L-Phe-OH

Guidance literature:: Multi-step reaction with 5 steps

1: n-BuLi / 1.) THF, hexane, -78 deg C, 20 min, 2.) -78 deg C, 15 min and room temp., 10 h

2: 1.) KHMDS, 2.) trisyl azide / 1.) THF, toluene, -78 deg C, 30 min, 2.) THF, -78 deg C, 2 min

3: H₂, 5 N HCl / 10percent Pd-C / tetrahydrofuran; methanol / 8 h / 760 Torr / Ambient temperature

4: K₂CO₃ / tetrahydrofuran; H₂O / Ambient temperature

5: 77 percent / aq. LiOH / tetrahydrofuran / 1 h / 0 °C

With hydrogenchloride; lithium hydroxide; n-butyllithium; 2,4,6-Triisopropylbenzenesulfonyl azide; hydrogen; potassium hexamethylsilazane; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; water;
DOI:10.1021/jo00088a009