[1,1'-Biphenyl]-3-ylhydrazine hydrochloride

Base Information

• Chemical Name: [1,1'-Biphenyl]-3-ylhydrazine hydrochloride
• CAS No.: 109221-88-7
• Molecular Formula: C₁₂H₁₂N₂*ClH
• Molecular Weight: 220.702
• Hs Code.: 2928000090
• DSSTox Substance ID: DTXSID20484242
• Mol file: 109221-88-7.mol

Synonyms:109221-88-7;[1,1'-Biphenyl]-3-ylhydrazine hydrochloride;BIPHENYL-3-YL-HYDRAZINE HYDROCHLORIDE;(3-phenylphenyl)hydrazine hydrochloride;(3-phenylphenyl)hydrazine;hydrochloride;[1,1'-Biphenyl]-3-ylhydrazine HCl;Hydrazine, [1,1'-biphenyl]-3-yl-, monohydrochloride;SCHEMBL4371464;DTXSID20484242;(3-phenylphenyl)diazane hydrochloride;MFCD06738781;AKOS016010034;AB27879;DS-6258;[1,1'-Biphenyl]-3-ylhydrazinehydrochloride;CS-0156450;C71323;A801980;Biphenyl-3-yl-hydrazine hydrochloride, AldrichCPR;([1,1'-Biphenyl]-3-yl)hydrazine--hydrogen chloride (1/1)

Chemical Property of [1,1'-Biphenyl]-3-ylhydrazine hydrochloride

Chemical Property:

• PSA: 38.05000
• LogP: 4.21450
• Storage Temp.: Inert atmosphere,Room Temperature
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 220.0767261
• Heavy Atom Count: 15
• Complexity: 164

Purity/Quality:

97% ^*data from raw suppliers

Biphenyl-3-yl-hydrazineHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C2=CC(=CC=C2)NN.Cl

Technology Process of [1,1'-Biphenyl]-3-ylhydrazine hydrochloride

There total 5 articles about [1,1'-Biphenyl]-3-ylhydrazine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.5%

C12H10N2*(x)ClH → [1,1'-biphenyl]-3-ylhydrazine hydrochloride (109221-88-7)

Guidance literature:

C₁₂H₁₀N₂*(x)ClH; With palladium on activated charcoal; hydrogen; at 100 ℃; for 7h; under 30003 Torr;

With hydrogenchloride; In water; at 100 ℃; for 2h;

Reference yield: 75.0%

3-bromobiphenyl (2113-57-7) → [1,1'-biphenyl]-3-ylhydrazine hydrochloride (109221-88-7)

Guidance literature:

3-bromobiphenyl; With potassium phosphate; copper(l) iodide; N,N′-bis(2,6-dimethylphenyl)oxalamide; cetyltrimethylammonim bromide; In water; at 80 ℃; for 0.25h; Schlenk technique; Inert atmosphere; Sealed tube;

With hydrazine hydrate; In water; at 80 ℃; Inert atmosphere; Schlenk technique; Sealed tube;

With hydrogenchloride; In water; pH=3 - 4; Inert atmosphere; Schlenk technique; Sealed tube;

DOI:10.1002/cjoc.201800326

Reference yield:

3-nitro-1,1'-biphenyl (2113-58-8) → [1,1'-biphenyl]-3-ylhydrazine hydrochloride (109221-88-7)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / Pd/C

2: SnCl₂ / H₂O

With hydrogen; tin(ll) chloride; palladium on activated charcoal; In water;

DOI:10.1016/S0960-894X(96)00263-6

upstream raw materials:

3-biphenyl amine

3-nitro-1,1'-biphenyl

3-bromobiphenyl

Downstream raw materials:

6-phenyl-2,3,3-trimethylindolenine

C₂₃H₁₇NO₃

9-(phenyl)-2-hydroxy-5,11-dihydro-6H-benzo[a]carbazole-3-carboxylic acid

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