N-tert-butoxycarbonyl-L-leucyl-L-(α-O-benzylaspartyl)-L-valine benzyl ester

Base Information

Chemical Name:N-tert-butoxycarbonyl-L-leucyl-L-(α-O-benzylaspartyl)-L-valine benzyl ester
CAS No.:224577-03-1
Molecular Formula:C₃₄H₄₇N₃O₈
Molecular Weight:625.762
Hs Code.:

Synonyms:N-tert-butoxycarbonyl-L-leucyl-L-(α-O-benzylaspartyl)-L-valine benzyl ester

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Chemical Property of N-tert-butoxycarbonyl-L-leucyl-L-(α-O-benzylaspartyl)-L-valine benzyl ester

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Technology Process of N-tert-butoxycarbonyl-L-leucyl-L-(α-O-benzylaspartyl)-L-valine benzyl ester

There total 4 articles about N-tert-butoxycarbonyl-L-leucyl-L-(α-O-benzylaspartyl)-L-valine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 3392-09-4
Boc-Leu-ONSu

: L-(α-O-benzylaspartyl)-L-O-benzylvaline hydrochloride

: 224577-03-1
N-tert-butoxycarbonyl-L-leucyl-L-(α-O-benzylaspartyl)-L-valine benzyl ester

Guidance literature:: With triethylamine; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1021/jm980673g

Reference yield:

: 13798-75-9
N^α-t-butoxycarbonylaspartic acid α-N-hydroxysuccinimide ester β-benzyl ester

: 224577-03-1
N-tert-butoxycarbonyl-L-leucyl-L-(α-O-benzylaspartyl)-L-valine benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

2: 4 M HCl / dioxane / 2 h / Ambient temperature

3: 86 percent / Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

With hydrogenchloride; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1021/jm980673g

Reference yield:

: 2462-34-2
L-valine benzyl ester hydrochloride

: 224577-03-1
N-tert-butoxycarbonyl-L-leucyl-L-(α-O-benzylaspartyl)-L-valine benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

2: 4 M HCl / dioxane / 2 h / Ambient temperature

3: 86 percent / Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

With hydrogenchloride; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1021/jm980673g