(2-dimethylamino-5-methylphenyl)tris(trimethylsilyl)silylmethanol

Base Information

• Chemical Name: (2-dimethylamino-5-methylphenyl)tris(trimethylsilyl)silylmethanol
• CAS No.: 269407-81-0
• Molecular Formula: C₁₉H₄₁NOSi₄
• Molecular Weight: 411.883
• Mol file: 269407-81-0.mol

Synonyms:(2-dimethylamino-5-methylphenyl)tris(trimethylsilyl)silylmethanol

Chemical Property of (2-dimethylamino-5-methylphenyl)tris(trimethylsilyl)silylmethanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2-dimethylamino-5-methylphenyl)tris(trimethylsilyl)silylmethanol

There total 1 articles about (2-dimethylamino-5-methylphenyl)tris(trimethylsilyl)silylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

2-(N,N-dimethylamino)-5-methylbenzaldehyde (64693-46-5) + tris(trimethylsilyl)silyl lithium * 3 tetrahydrofuran → (2-dimethylamino-5-methylphenyl)tris(trimethylsilyl)silylmethanol (269407-81-0)

Guidance literature:

tris(trimethylsilyl)silyl lithium * 3 tetrahydrofuran; With magnesium bromide; In diethyl ether; at 20 ℃; for 0.5h;

2-(N,N-dimethylamino)-5-methylbenzaldehyde; In diethyl ether; at -78 - 20 ℃;

DOI:10.1016/S0022-328X(99)00740-8

Reference yield: 63.0%

(2-dimethylamino-5-methylphenyl)tris(trimethylsilyl)silylmethanol (269407-81-0) → 1-(2-dimethylamino-5-methylbenzyl)-2-[2-dimethylamino-5-methyl-(α-trimethylsiloxy)benzyl]-1,1,2,2-tetrakis(trimethylsilyl)disilane

Guidance literature:

With triethylborane-tetrahydrofuran; methyllithium; In diethyl ether; at -78 - 20 ℃;

DOI:10.1016/S0022-328X(99)00740-8

Reference yield:

(2-dimethylamino-5-methylphenyl)tris(trimethylsilyl)silylmethanol (269407-81-0) → (E)-2,4-bis(2-dimethylamino-5-methylphenyl)-1,1,3,3-tetrakis(trimethylsilyl)-1,3-disilacyclobutane

Guidance literature:

With methyllithium; In diethyl ether; at -78 - 20 ℃;

DOI:10.1016/S0022-328X(99)00740-8

upstream raw materials:

2-(N,N-dimethylamino)-5-methylbenzaldehyde