tert-butyl [(2E)-2-amino-1-[(benzyloxy)methyl]-2-(hydroxyimino)ethyl]carbamate

Base Information

Chemical Name:tert-butyl [(2E)-2-amino-1-[(benzyloxy)methyl]-2-(hydroxyimino)ethyl]carbamate
CAS No.:911639-71-9
Molecular Formula:C₁₅H₂₃N₃O₄
Molecular Weight:309.365
Hs Code.:

Synonyms:tert-butyl [(2E)-2-amino-1-[(benzyloxy)methyl]-2-(hydroxyimino)ethyl]carbamate

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Chemical Property of tert-butyl [(2E)-2-amino-1-[(benzyloxy)methyl]-2-(hydroxyimino)ethyl]carbamate

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Technology Process of tert-butyl [(2E)-2-amino-1-[(benzyloxy)methyl]-2-(hydroxyimino)ethyl]carbamate

There total 1 articles about tert-butyl [(2E)-2-amino-1-[(benzyloxy)methyl]-2-(hydroxyimino)ethyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 911494-53-6
tert-butyl [2-(benzyloxy)-1-cyanoethyl]carbamate

: 911639-71-9
tert-butyl [(2E)-2-amino-1-[(benzyloxy)methyl]-2-(hydroxyimino)ethyl]carbamate

Guidance literature:: With potassium hydroxide; hydroxylamine hydrochloride; In methanol; for 0.25h;

tert-butyl [2-(benzyloxy)-1-cyanoethyl]carbamate; In methanol; at 45 ℃; for 17h;

Reference yield:

: 911639-71-9
tert-butyl [(2E)-2-amino-1-[(benzyloxy)methyl]-2-(hydroxyimino)ethyl]carbamate

: 911491-26-4
N-(4-fluorobenzyl)-3-hydroxy-9,9-dimethyl-4-oxo-6,7,8,9-tetrahydro-4H-pyrazino[1,2-a]pyrimidine-2-carboxamide

: 911494-24-1
methyl 5-(benzoyloxy)-2-{2-(benzyloxy)-1-[(tert-butoxycarbonyl)amino]ethyl}-6-hydroxypyrimidine-4-carboxylate

Guidance literature:: tert-butyl [(2E)-2-amino-1-[(benzyloxy)methyl]-2-(hydroxyimino)ethyl]carbamate; dimethyl acetylenedicarboxylate; In chloroform; xylene; at 145 ℃; for 26.5h; Heating / reflux;

N-(4-fluorobenzyl)-3-hydroxy-9,9-dimethyl-4-oxo-6,7,8,9-tetrahydro-4H-pyrazino[1,2-a]pyrimidine-2-carboxamide; With pyridine; In dichloromethane; at 20 ℃;

Reference yield:

: 911639-71-9
tert-butyl [(2E)-2-amino-1-[(benzyloxy)methyl]-2-(hydroxyimino)ethyl]carbamate

: C₂₃H₂₂ClFN₄O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: chloroform; xylene / 26.5 h / 145 °C / Heating / reflux

1.2: 20 °C

2.1: methanol / 24 h / Heating / reflux

3.1: dichloromethane / 1.5 h / 20 °C

4.1: triethylamine; trimethyl orthoformate / 2 h / 20 °C

With triethylamine; trimethyl orthoformate; In methanol; dichloromethane; chloroform; xylene;