trans-8-chloro-1-(4-isopropoxy-cyclohexyl)-4H,6H-5-oxa-2,3,10b-triaza-benzo[e]azulene

Base Information

Chemical Name:trans-8-chloro-1-(4-isopropoxy-cyclohexyl)-4H,6H-5-oxa-2,3,10b-triaza-benzo[e]azulene
CAS No.:1428523-46-9
Molecular Formula:C₁₉H₂₄ClN₃O₂
Molecular Weight:361.871
Hs Code.:

Synonyms:trans-8-chloro-1-(4-isopropoxy-cyclohexyl)-4H,6H-5-oxa-2,3,10b-triaza-benzo[e]azulene

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Chemical Property of trans-8-chloro-1-(4-isopropoxy-cyclohexyl)-4H,6H-5-oxa-2,3,10b-triaza-benzo[e]azulene

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Technology Process of trans-8-chloro-1-(4-isopropoxy-cyclohexyl)-4H,6H-5-oxa-2,3,10b-triaza-benzo[e]azulene

There total 6 articles about trans-8-chloro-1-(4-isopropoxy-cyclohexyl)-4H,6H-5-oxa-2,3,10b-triaza-benzo[e]azulene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1227187-86-1
trans-4-(isopropoxy)cyclohexanecarboxylic acid hydrazide

: 1428523-61-8
7-chloro-3,5-dihydrobenzo[e][1,4]oxazepine-2(1H)-thione

: 1428523-46-9
trans-8-chloro-1-(4-isopropoxy-cyclohexyl)-4H,6H-5-oxa-2,3,10b-triaza-benzo[e]azulene

Guidance literature:: In butan-1-ol; Reflux;

Reference yield:

: 1227187-59-8
trans-4-(isopropoxy)cyclohexanecarboxylic acid ethyl ester

: 1428523-46-9
trans-8-chloro-1-(4-isopropoxy-cyclohexyl)-4H,6H-5-oxa-2,3,10b-triaza-benzo[e]azulene

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / butan-1-ol / Reflux

2: butan-1-ol / Reflux

With hydrazine hydrate; In butan-1-ol;

Reference yield:

: 4-(trimethylsilanyloxy)cyclohexanecarboxylic acid ethyl ester

: 1428523-46-9
trans-8-chloro-1-(4-isopropoxy-cyclohexyl)-4H,6H-5-oxa-2,3,10b-triaza-benzo[e]azulene

Guidance literature:: Multi-step reaction with 3 steps

1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1 h / -78 °C

1.2: -78 - 20 °C

2.1: hydrazine hydrate / butan-1-ol / 72 h / Reflux

3.1: butan-1-ol / 72 h / Reflux

With trimethylsilyl trifluoromethanesulfonate; hydrazine hydrate; In dichloromethane; butan-1-ol;