C₁₂H₁₇NO

Base Information

• Chemical Name: C₁₂H₁₇NO
• CAS No.: 910095-61-3
• Molecular Formula: C₁₂H₁₇NO
• Molecular Weight: 191.273

Synonyms:C₁₂H₁₇NO

Chemical Property of C₁₂H₁₇NO

Chemical Property:

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Technology Process of C₁₂H₁₇NO

There total 3 articles about C₁₂H₁₇NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(3R,4R)-(1,4-dibenzylpyrrolidin-3-yl)methanol → C12H17NO (910095-61-3)

Guidance literature:

With palladium hydroxide, 20 wt% on carbon; In ethanol; at 20 ℃; for 16h; under 2250.23 Torr; Inert atmosphere;

DOI:10.1021/acs.orglett.6b00293

Reference yield:

ethyl 3-benzylacrylate (54966-42-6,1466-22-4) → C12H17NO (910095-61-3)

Guidance literature:

Multi-step reaction with 4 steps

1.1: toluene / 0.17 h / 0 °C / Inert atmosphere

1.2: 1.25 h / 0 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.75 h / 0 °C

2.2: 1 h

3.1: ammonia / methanol / Resolution of racemate

4.1: palladium hydroxide, 20 wt% on carbon / ethanol / 16 h / 20 °C / 2250.23 Torr / Inert atmosphere

With lithium aluminium tetrahydride; palladium hydroxide, 20 wt% on carbon; ammonia; In tetrahydrofuran; methanol; diethyl ether; ethanol; toluene;

DOI:10.1021/acs.orglett.6b00293

Reference yield:

(3SR,4SR)-1,4-dibenzyl-pyrrolidine-3-carboxylic acid ethyl ester → C12H17NO (910095-61-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0.75 h / 0 °C

1.2: 1 h

2.1: ammonia / methanol / Resolution of racemate

3.1: palladium hydroxide, 20 wt% on carbon / ethanol / 16 h / 20 °C / 2250.23 Torr / Inert atmosphere

With lithium aluminium tetrahydride; palladium hydroxide, 20 wt% on carbon; ammonia; In tetrahydrofuran; methanol; diethyl ether; ethanol;

DOI:10.1021/acs.orglett.6b00293

upstream raw materials:

ethyl 3-benzylacrylate

Downstream raw materials:

(3R,4R)-3-benzyl-4-hydroxymethylpyrrolidine-1-carboxylic acid tert-butyl ester

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