1-D-6-O-(2-amino-2-deoxy-α-D-glucopyranosyl)-2-O-methyl-myo-inositol 1-(acetoxymethyl octadecyl phosphate)

Base Information

Chemical Name:1-D-6-O-(2-amino-2-deoxy-α-D-glucopyranosyl)-2-O-methyl-myo-inositol 1-(acetoxymethyl octadecyl phosphate)
CAS No.:827574-38-9
Molecular Formula:C₃₄H₆₆NO₁₅P
Molecular Weight:759.869
Hs Code.:

Synonyms:1-D-6-O-(2-amino-2-deoxy-α-D-glucopyranosyl)-2-O-methyl-myo-inositol 1-(acetoxymethyl octadecyl phosphate)

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Chemical Property of 1-D-6-O-(2-amino-2-deoxy-α-D-glucopyranosyl)-2-O-methyl-myo-inositol 1-(acetoxymethyl octadecyl phosphate)

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Technology Process of 1-D-6-O-(2-amino-2-deoxy-α-D-glucopyranosyl)-2-O-methyl-myo-inositol 1-(acetoxymethyl octadecyl phosphate)

There total 4 articles about 1-D-6-O-(2-amino-2-deoxy-α-D-glucopyranosyl)-2-O-methyl-myo-inositol 1-(acetoxymethyl octadecyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 869192-46-1
1-D-6-O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-3,4,5-tri-O-benzyl-2-O-methyl-myo-inositol 1-(acetoxymethyl octadecyl phosphate)

: 827574-38-9
1-D-6-O-(2-amino-2-deoxy-α-D-glucopyranosyl)-2-O-methyl-myo-inositol 1-(acetoxymethyl octadecyl phosphate)

Guidance literature:: With hydrogen; palladium dihydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 2h; under 2280 Torr;
DOI:10.1016/j.tetlet.2005.08.112

Reference yield:

: tetraethylammonium 1-D-6-O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-3,4,5-tri-O-benzyl-2-O-methyl-myo-inositol 1-(octadecyl phosphate)

: 827574-38-9
1-D-6-O-(2-amino-2-deoxy-α-D-glucopyranosyl)-2-O-methyl-myo-inositol 1-(acetoxymethyl octadecyl phosphate)

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / DIEA / tetrahydrofuran / 20 °C

2: 96 percent / H₂ / Pd(OH)2/C / tetrahydrofuran; methanol / 2 h / 20 °C / 2280 Torr

With hydrogen; N-ethyl-N,N-diisopropylamine; palladium dihydroxide; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetlet.2005.08.112

Reference yield:

: 197369-80-5
1D-6-O-(2-Azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-3,4,5-tri-O-benzyl-2-O-methyl-myo-inositol

: 827574-38-9
1-D-6-O-(2-amino-2-deoxy-α-D-glucopyranosyl)-2-O-methyl-myo-inositol 1-(acetoxymethyl octadecyl phosphate)

Guidance literature:: Multi-step reaction with 3 steps

1.1: pivaloyl chloride / pyridine / 1 h / 20 °C

1.2: 80 percent / iodine / pyridine; H₂O / 0.75 h / 20 °C

2.1: 94 percent / DIEA / tetrahydrofuran / 20 °C

3.1: 96 percent / H₂ / Pd(OH)2/C / tetrahydrofuran; methanol / 2 h / 20 °C / 2280 Torr

With hydrogen; pivaloyl chloride; N-ethyl-N,N-diisopropylamine; palladium dihydroxide; In tetrahydrofuran; pyridine; methanol;
DOI:10.1016/j.tetlet.2005.08.112