Ethenesulfonic acid ((S)-2-cyclohexa-1,3-dienyl-1-methyl-ethyl)-((S)-1-phenyl-ethyl)-amide

Base Information

• Chemical Name: Ethenesulfonic acid ((S)-2-cyclohexa-1,3-dienyl-1-methyl-ethyl)-((S)-1-phenyl-ethyl)-amide
• CAS No.: 882426-41-7
• Molecular Formula: C₁₉H₂₅NO₂S
• Molecular Weight: 331.479

Synonyms:Ethenesulfonic acid ((S)-2-cyclohexa-1,3-dienyl-1-methyl-ethyl)-((S)-1-phenyl-ethyl)-amide

Chemical Property of Ethenesulfonic acid ((S)-2-cyclohexa-1,3-dienyl-1-methyl-ethyl)-((S)-1-phenyl-ethyl)-amide

Chemical Property:

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Technology Process of Ethenesulfonic acid ((S)-2-cyclohexa-1,3-dienyl-1-methyl-ethyl)-((S)-1-phenyl-ethyl)-amide

There total 4 articles about Ethenesulfonic acid ((S)-2-cyclohexa-1,3-dienyl-1-methyl-ethyl)-((S)-1-phenyl-ethyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

((S)-2-Cyclohexa-1,3-dienyl-1-methyl-ethyl)-((S)-1-phenyl-ethyl)-amine (882426-39-3) + vinylsulfonyl chloride (6608-47-5) → Ethenesulfonic acid ((S)-2-cyclohexa-1,3-dienyl-1-methyl-ethyl)-((S)-1-phenyl-ethyl)-amide (882426-41-7)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃; for 3h;

DOI:10.3987/COM-05-S(T)80

Reference yield:

methanesulfonic acid 2-cyclohexa-1,3-dienyl-1-methyl-ethyl ester (265116-11-8) → Ethenesulfonic acid ((S)-2-cyclohexa-1,3-dienyl-1-methyl-ethyl)-((S)-1-phenyl-ethyl)-amide (882426-41-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 12 h / 80 °C

2: 79 percent / Et₃N / CH₂Cl₂ / 3 h / 0 °C

With triethylamine; In dichloromethane;

DOI:10.3987/COM-05-S(T)80

Reference yield:

(S)-1-phenyl-ethylamine (2627-86-3) → Ethenesulfonic acid ((S)-2-cyclohexa-1,3-dienyl-1-methyl-ethyl)-((S)-1-phenyl-ethyl)-amide (882426-41-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 12 h / 80 °C

2: 79 percent / Et₃N / CH₂Cl₂ / 3 h / 0 °C

With triethylamine; In dichloromethane;

DOI:10.3987/COM-05-S(T)80

upstream raw materials:

((S)-2-Cyclohexa-1,3-dienyl-1-methyl-ethyl)-((S)-1-phenyl-ethyl)-amine

vinylsulfonyl chloride

methanesulfonic acid 2-cyclohexa-1,3-dienyl-1-methyl-ethyl ester

(S)-1-phenyl-ethylamine

Downstream raw materials:

(1R,3S,6S,8S)-3-Methyl-4-((S)-1-phenyl-ethyl)-5-thia-4-aza-tricyclo[6.2.2.0^1,6]dodec-9-ene 5,5-dioxide

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