4,5-dihydro-2,1,3-benzoxadiazole-4,5-dione 4-(2,4-dinitrophenylhydrazone) 5-oxime

Base Information

Chemical Name:4,5-dihydro-2,1,3-benzoxadiazole-4,5-dione 4-(2,4-dinitrophenylhydrazone) 5-oxime
CAS No.:1254183-63-5
Molecular Formula:C₁₂H₇N₇O₆
Molecular Weight:345.231
Hs Code.:

Synonyms:4,5-dihydro-2,1,3-benzoxadiazole-4,5-dione 4-(2,4-dinitrophenylhydrazone) 5-oxime

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Chemical Property of 4,5-dihydro-2,1,3-benzoxadiazole-4,5-dione 4-(2,4-dinitrophenylhydrazone) 5-oxime

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Technology Process of 4,5-dihydro-2,1,3-benzoxadiazole-4,5-dione 4-(2,4-dinitrophenylhydrazone) 5-oxime

There total 5 articles about 4,5-dihydro-2,1,3-benzoxadiazole-4,5-dione 4-(2,4-dinitrophenylhydrazone) 5-oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.3%

: 4-Hydroxy-5-nitrosobenzo-2,1,3-oxadiazol

: 119-26-6
(2,4-dinitro-phenyl)-hydrazine

: 1254183-63-5
4,5-dihydro-2,1,3-benzoxadiazole-4,5-dione 4-(2,4-dinitrophenylhydrazone) 5-oxime

Guidance literature:: With hydrogenchloride; In methanol; at 20 ℃; for 8h;
DOI:10.1007/s11172-009-0329-3

Reference yield:

: 118-02-5
2,4-dinitrosoresorcinol

: 1254183-63-5
4,5-dihydro-2,1,3-benzoxadiazole-4,5-dione 4-(2,4-dinitrophenylhydrazone) 5-oxime

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride; hydroxylamine hydrochloride / ethanol; water / 2 h / Reflux

2: acetic anhydride / 1 h / 80 - 90 °C

3: hydrogenchloride / water; methanol / 1 h / Reflux

4: hydrogenchloride / methanol / 8 h / 20 °C

With hydrogenchloride; hydroxylamine hydrochloride; acetic anhydride; In methanol; ethanol; water;
DOI:10.1007/s11172-009-0329-3

Reference yield:

: 108-46-3
recorcinol

: 1254183-63-5
4,5-dihydro-2,1,3-benzoxadiazole-4,5-dione 4-(2,4-dinitrophenylhydrazone) 5-oxime

Guidance literature:: Multi-step reaction with 5 steps

1: sodium nitrite; sulfuric acid

2: hydrogenchloride; hydroxylamine hydrochloride / ethanol; water / 2 h / Reflux

3: acetic anhydride / 1 h / 80 - 90 °C

4: hydrogenchloride / water; methanol / 1 h / Reflux

5: hydrogenchloride / methanol / 8 h / 20 °C

With hydrogenchloride; sulfuric acid; hydroxylamine hydrochloride; acetic anhydride; sodium nitrite; In methanol; ethanol; water;
DOI:10.1007/s11172-009-0329-3