sodium 2-{4-[3-(4-chlorophenyl)-4-pyrimidin-4-yl-1H-pyrazol-5-yl]piperidin-1-yl}-2-oxoethyl hydrogen phosphate

Base Information

Chemical Name:sodium 2-{4-[3-(4-chlorophenyl)-4-pyrimidin-4-yl-1H-pyrazol-5-yl]piperidin-1-yl}-2-oxoethyl hydrogen phosphate
CAS No.:635725-11-0
Molecular Formula:C₂₀H₂₀ClN₅O₅P*Na
Molecular Weight:499.826
Hs Code.:

Synonyms:sodium 2-{4-[3-(4-chlorophenyl)-4-pyrimidin-4-yl-1H-pyrazol-5-yl]piperidin-1-yl}-2-oxoethyl hydrogen phosphate

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Chemical Property of sodium 2-{4-[3-(4-chlorophenyl)-4-pyrimidin-4-yl-1H-pyrazol-5-yl]piperidin-1-yl}-2-oxoethyl hydrogen phosphate

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Technology Process of sodium 2-{4-[3-(4-chlorophenyl)-4-pyrimidin-4-yl-1H-pyrazol-5-yl]piperidin-1-yl}-2-oxoethyl hydrogen phosphate

There total 3 articles about sodium 2-{4-[3-(4-chlorophenyl)-4-pyrimidin-4-yl-1H-pyrazol-5-yl]piperidin-1-yl}-2-oxoethyl hydrogen phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 635725-10-9
2-{4-[3-(4-chlorophenyl)-4-pyrimidin-4-yl-1H-pyrazol-5-yl]piperidin-1-yl}-2-oxoethyl dihydrogen phosphate

: 635725-11-0
sodium 2-{4-[3-(4-chlorophenyl)-4-pyrimidin-4-yl-1H-pyrazol-5-yl]piperidin-1-yl}-2-oxoethyl hydrogen phosphate

Guidance literature:: With sodium hydroxide; In water; for 0.25h;

Reference yield:

: di(tert-butyl) 2-{4-[3-(4-chlorophenyl)-4-pyrimidin-4-yl-1H-pyrazol-5-yl]piperidin-1-yl}-2-oxoethyl phosphate

: 635725-11-0
sodium 2-{4-[3-(4-chlorophenyl)-4-pyrimidin-4-yl-1H-pyrazol-5-yl]piperidin-1-yl}-2-oxoethyl hydrogen phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / 1,4-dioxane; water / 20 °C

2: sodium hydroxide / water / 0.25 h

With sodium hydroxide; trifluoroacetic acid; In 1,4-dioxane; water;

Reference yield:

: 271576-80-8,1184301-42-5
2-{4-[3-(4-chlorophenyl)-4-pyrimidin-4-yl-1H-pyrazol-5-yl]piperidin-1-yl}-2-oxoethanol

: 635725-11-0
sodium 2-{4-[3-(4-chlorophenyl)-4-pyrimidin-4-yl-1H-pyrazol-5-yl]piperidin-1-yl}-2-oxoethyl hydrogen phosphate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1H-tetrazole / tetrahydrofuran / 1 h / 20 °C

1.2: monomethylmagnesium perphthalate (MMPP) / 0 - 20 °C

2.1: trifluoroacetic acid / 1,4-dioxane; water / 20 °C

3.1: sodium hydroxide / water / 0.25 h

With 1H-tetrazole; sodium hydroxide; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; water;