Technology Process of Methyl 2-iodo-3-methoxybenzeneacetate
There total 4 articles about Methyl 2-iodo-3-methoxybenzeneacetate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride; potassium iodide; sodium nitrite;
In
water;
at -5 - 20 ℃;
for 20h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: H2 / Pd/C / methanol / 5 h / 45 °C
2: NaNO2; HCl; KI / H2O / 20 h / -5 - 20 °C
With
hydrogenchloride; hydrogen; potassium iodide; sodium nitrite;
palladium on activated charcoal;
In
methanol; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / dimethylformamide / 20 °C
1.2: 80 percent / H2O2; aq. NaOH / cooling
2.1: 100 percent / diethyl ether / 20 °C
3.1: H2 / Pd/C / methanol / 5 h / 45 °C
4.1: NaNO2; HCl; KI / H2O / 20 h / -5 - 20 °C
With
hydrogenchloride; hydrogen; sodium hydride; potassium iodide; sodium nitrite;
palladium on activated charcoal;
In
methanol; diethyl ether; water; N,N-dimethyl-formamide;