(3R,4R,5S)-4-(4-methoxyphenyl)-1-(toluene-4-sulfonyl)-5-triisopropyl-silanyloxy-piperidin-3-ol

Base Information

Chemical Name:(3R,4R,5S)-4-(4-methoxyphenyl)-1-(toluene-4-sulfonyl)-5-triisopropyl-silanyloxy-piperidin-3-ol
CAS No.:944952-82-3
Molecular Formula:C₂₈H₄₃NO₅SSi
Molecular Weight:533.805
Hs Code.:

Synonyms:(3R,4R,5S)-4-(4-methoxyphenyl)-1-(toluene-4-sulfonyl)-5-triisopropyl-silanyloxy-piperidin-3-ol

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Chemical Property of (3R,4R,5S)-4-(4-methoxyphenyl)-1-(toluene-4-sulfonyl)-5-triisopropyl-silanyloxy-piperidin-3-ol

Chemical Property:

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Technology Process of (3R,4R,5S)-4-(4-methoxyphenyl)-1-(toluene-4-sulfonyl)-5-triisopropyl-silanyloxy-piperidin-3-ol

There total 2 articles about (3R,4R,5S)-4-(4-methoxyphenyl)-1-(toluene-4-sulfonyl)-5-triisopropyl-silanyloxy-piperidin-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 944952-84-5
(3R,4R,5S)-4-(4-hydroxyphenyl)-1-(toluene-4-sulfonyl)-5-triisopropylsilanyloxypiperidin-3-ol

: 77-78-1
dimethyl sulfate

: 944952-82-3
(3R,4R,5S)-4-(4-methoxyphenyl)-1-(toluene-4-sulfonyl)-5-triisopropyl-silanyloxy-piperidin-3-ol

Guidance literature:: With potassium carbonate; In acetone; at 80 ℃; for 24h;

Reference yield:

: 944952-84-5
(3R,4R,5S)-4-(4-hydroxyphenyl)-1-(toluene-4-sulfonyl)-5-triisopropylsilanyloxypiperidin-3-ol

: of tert-butyl methyl ether

: 944952-82-3
(3R,4R,5S)-4-(4-methoxyphenyl)-1-(toluene-4-sulfonyl)-5-triisopropyl-silanyloxy-piperidin-3-ol

Guidance literature:: With potassium carbonate; dimethyl sulfate; In water; acetone;

Reference yield:

: 857272-02-7
6-chloromethyl-4-(3-methoxy-propyl)-4H-benzo[1,4]oxazin-3-one

: 944952-82-3
(3R,4R,5S)-4-(4-methoxyphenyl)-1-(toluene-4-sulfonyl)-5-triisopropyl-silanyloxy-piperidin-3-ol

: 944952-80-1
6-[(3R,4R,5S)-4-(4-methoxyphenyl)-1-(toluene-4-sulfonyl)-5-triisopropylsilanyloxypiperidin-3-yloxymethyl]-4-(3-methoxypropyl)-4H-benzo[1,4]oxazin-3-one

Guidance literature:: 6-chloromethyl-4-(3-methoxy-propyl)-4H-benzo[1,4]oxazin-3-one; (3R,4R,5S)-4-(4-methoxyphenyl)-1-(toluene-4-sulfonyl)-5-triisopropyl-silanyloxy-piperidin-3-ol; With sodium hydride; In N,N-dimethyl-formamide; at -10 - 20 ℃; for 19h;

With water; sodium hydrogencarbonate; In N,N-dimethyl-formamide;