Technology Process of C50H58N8O2
There total 5 articles about C50H58N8O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl-formamide; paraffin oil / 1 h / 0 - 20 °C
1.2: 36 h / 90 °C
2.1: trifluoroacetic acid / dichloromethane / 20 °C
3.1: trichlorophosphate / toluene / 2 h / Inert atmosphere; Reflux
With
sodium hydride; trifluoroacetic acid; trichlorophosphate;
In
dichloromethane; N,N-dimethyl-formamide; toluene; paraffin oil;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / acetone / Reflux
2: potassium tert-butylate / tert-Amyl alcohol / 9 h / Inert atmosphere; Reflux
3: trichlorophosphate / toluene / 2 h / Inert atmosphere; Reflux
With
potassium tert-butylate; potassium carbonate; trichlorophosphate;
In
tert-Amyl alcohol; acetone; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium tert-butylate / tert-Amyl alcohol / 9 h / Inert atmosphere; Reflux
2: trichlorophosphate / toluene / 2 h / Inert atmosphere; Reflux
With
potassium tert-butylate; trichlorophosphate;
In
tert-Amyl alcohol; toluene;