Boc-D-Glu-NH2

Base Information

Chemical Name:Boc-D-Glu-NH2
CAS No.:130457-45-3
Molecular Formula:C₂₆H₄₁N₅O₇
Molecular Weight:535.641
Hs Code.:

Synonyms:Boc-D-Glu-NH2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Boc-D-Glu-NH2

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Technology Process of Boc-D-Glu-NH2

There total 1 articles about Boc-D-Glu-NH2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 55227-02-6
Boc-D-Glu(OSu)-NH₂

: 66397-86-2
H-Lys(Z)-NHEt

: 130457-45-3
Boc-D-Glu-NH2

Guidance literature:: With TEA; In 1,2-dimethoxyethane; water; Ambient temperature;
DOI:10.1016/S0040-4020(01)86764-8

Reference yield: 96.0%

: 130457-45-3
Boc-D-Glu-NH2

: 130457-46-4
H-D-Glu-NH2*HCl

Guidance literature:: With hydrogenchloride; acetic acid; for 0.333333h;
DOI:10.1016/S0040-4020(01)86764-8

Reference yield:

: 130457-45-3
Boc-D-Glu-NH2

: 130457-48-6
H-Ala-D-Glu-NH2*HCl

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / AcOH, 1.8N HCl / 0.33 h

2: 1) HOBt*H₂O, DCCI, 2) 4.3N HCl / 1) DMF, -10 deg C, 1h, r.t., overnight, 2) DMF, 20 min

With hydrogenchloride; benzotriazol-1-ol; acetic acid; dicyclohexyl-carbodiimide;
DOI:10.1016/S0040-4020(01)86764-8