N-Allyl-N-[2-(1-chloro-2,2-bis-methylsulfanyl-vinyl)-4-methyl-phenyl]-4-methyl-benzenesulfonamide

Base Information

Chemical Name:N-Allyl-N-[2-(1-chloro-2,2-bis-methylsulfanyl-vinyl)-4-methyl-phenyl]-4-methyl-benzenesulfonamide
CAS No.:132353-95-8
Molecular Formula:C₂₁H₂₄ClNO₂S₃
Molecular Weight:454.078
Hs Code.:

Synonyms:N-Allyl-N-[2-(1-chloro-2,2-bis-methylsulfanyl-vinyl)-4-methyl-phenyl]-4-methyl-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Allyl-N-[2-(1-chloro-2,2-bis-methylsulfanyl-vinyl)-4-methyl-phenyl]-4-methyl-benzenesulfonamide

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Technology Process of N-Allyl-N-[2-(1-chloro-2,2-bis-methylsulfanyl-vinyl)-4-methyl-phenyl]-4-methyl-benzenesulfonamide

There total 7 articles about N-Allyl-N-[2-(1-chloro-2,2-bis-methylsulfanyl-vinyl)-4-methyl-phenyl]-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: (E)-N-<2-(2-methylthio-2-methylsulphinylvinyl)-4-methylphenyl>-N-(prop-2-enyl)toluene-4-sulphonamide

: 132353-95-8
N-Allyl-N-[2-(1-chloro-2,2-bis-methylsulfanyl-vinyl)-4-methyl-phenyl]-4-methyl-benzenesulfonamide

Guidance literature:: With hydrogenchloride; In dichloromethane; for 2h;

Reference yield:

: 2941-78-8
2-Amino-5-methylbenzoic acid

: 132353-95-8
N-Allyl-N-[2-(1-chloro-2,2-bis-methylsulfanyl-vinyl)-4-methyl-phenyl]-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 6 steps

1: 100 percent / Na₂CO₃ / H₂O / 0.33 h / 70 °C

2: LiAlH₄ / tetrahydrofuran / 1 h / Heating

3: 93.4 percent / pyridinium chlorochromate / CH₂Cl₂ / 3 h

4: 77 percent / Triton B / tetrahydrofuran / 60 h / Heating

5: 1) NaH / 1) DMF, 5 min; 2) 40 deg C, 10 min

6: 100 percent / 10M aq. HCl / CH₂Cl₂ / 2 h

With hydrogenchloride; lithium aluminium tetrahydride; N-benzyl-trimethylammonium hydroxide; sodium hydride; sodium carbonate; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; water;

Reference yield:

: 34161-85-8
N-(2-formyl-4-methylphenyl)-4-methylbenzenesulfonamide

: 132353-95-8
N-Allyl-N-[2-(1-chloro-2,2-bis-methylsulfanyl-vinyl)-4-methyl-phenyl]-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / Triton B / tetrahydrofuran / 60 h / Heating

2: 1) NaH / 1) DMF, 5 min; 2) 40 deg C, 10 min

3: 100 percent / 10M aq. HCl / CH₂Cl₂ / 2 h

With hydrogenchloride; N-benzyl-trimethylammonium hydroxide; sodium hydride; In tetrahydrofuran; dichloromethane;