Carbonic acid 3-allyl-5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-ylmethyl ester benzyl ester

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Chemical Name:Carbonic acid 3-allyl-5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-ylmethyl ester benzyl ester
CAS No.:118004-24-3
Molecular Formula:C₁₆H₁₅FN₂O₅
Molecular Weight:334.304
Hs Code.:

Synonyms:Carbonic acid 3-allyl-5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-ylmethyl ester benzyl ester

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Chemical Property of Carbonic acid 3-allyl-5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-ylmethyl ester benzyl ester

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Technology Process of Carbonic acid 3-allyl-5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-ylmethyl ester benzyl ester

There total 3 articles about Carbonic acid 3-allyl-5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-ylmethyl ester benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 116097-53-1
1-(benzyloxycarbonyloxymethyl)-5-fluorouracil

: 106-95-6
allyl bromide

: 118004-24-3
Carbonic acid 3-allyl-5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-ylmethyl ester benzyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile;
DOI:10.1246/cl.1988.1381

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 118004-24-3
Carbonic acid 3-allyl-5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-ylmethyl ester benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / triethylamine / acetonitrile

2: 96 percent / ethyldiisopropylamine (EDA) / acetonitrile

With triethylamine; N-ethyl-N,N-diisopropylamine; In acetonitrile;
DOI:10.1246/cl.1988.1381

Reference yield:

: 74179-14-9
N¹,N³-bis(hydroxymethyl)-5-fluorouracil

: 118004-24-3
Carbonic acid 3-allyl-5-fluoro-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-ylmethyl ester benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / triethylamine / acetonitrile

2: 96 percent / ethyldiisopropylamine (EDA) / acetonitrile

With triethylamine; N-ethyl-N,N-diisopropylamine; In acetonitrile;
DOI:10.1246/cl.1988.1381