2-{4-[3-methanesulfonyl-1-(4-methoxyphenyl)-7-oxo-1,4,5,7-tetrahydropyrazolo[3,4-c]pyridin-6-yl]phenyl}-2-methylpropionic acid methyl ester

Base Information

• Chemical Name: 2-{4-[3-methanesulfonyl-1-(4-methoxyphenyl)-7-oxo-1,4,5,7-tetrahydropyrazolo[3,4-c]pyridin-6-yl]phenyl}-2-methylpropionic acid methyl ester
• CAS No.: 630383-89-0
• Molecular Formula: C₂₅H₂₇N₃O₆S
• Molecular Weight: 497.572

Synonyms:2-{4-[3-methanesulfonyl-1-(4-methoxyphenyl)-7-oxo-1,4,5,7-tetrahydropyrazolo[3,4-c]pyridin-6-yl]phenyl}-2-methylpropionic acid methyl ester

Chemical Property of 2-{4-[3-methanesulfonyl-1-(4-methoxyphenyl)-7-oxo-1,4,5,7-tetrahydropyrazolo[3,4-c]pyridin-6-yl]phenyl}-2-methylpropionic acid methyl ester

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Technology Process of 2-{4-[3-methanesulfonyl-1-(4-methoxyphenyl)-7-oxo-1,4,5,7-tetrahydropyrazolo[3,4-c]pyridin-6-yl]phenyl}-2-methylpropionic acid methyl ester

There total 2 articles about 2-{4-[3-methanesulfonyl-1-(4-methoxyphenyl)-7-oxo-1,4,5,7-tetrahydropyrazolo[3,4-c]pyridin-6-yl]phenyl}-2-methylpropionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

1-(4-methoxyphenyl)-3-(methylsulfonyl)-1,4,5,6-tetrahydro-7H-pyrazolo[3,4-c]pyridin-7-one (630383-13-0) + 2-(4-Iodo-phenyl)-2-methyl-propionic acid methyl ester (630383-83-4) → 2-{4-[3-methanesulfonyl-1-(4-methoxyphenyl)-7-oxo-1,4,5,7-tetrahydropyrazolo[3,4-c]pyridin-6-yl]phenyl}-2-methylpropionic acid methyl ester (630383-89-0)

Guidance literature:

With copper(l) iodide; 1,10-Phenanthroline; potassium carbonate; In dimethyl sulfoxide; at 130 ℃;

DOI:10.1016/j.bmcl.2014.05.101

Reference yield: 45.9%

1-(4-methoxyphenyl)-7-oxo-4,5,6,7-tetrahydro-1H-pyrazolo[3, 4-c]pyridine-3-carboxylic acid ethyl ester (503614-56-0) + 2-(4-Iodo-phenyl)-2-methyl-propionic acid methyl ester (630383-83-4) → 2-{4-[3-methanesulfonyl-1-(4-methoxyphenyl)-7-oxo-1,4,5,7-tetrahydropyrazolo[3,4-c]pyridin-6-yl]phenyl}-2-methylpropionic acid methyl ester (630383-89-0)

Guidance literature:

With copper(l) iodide; potassium carbonate; In dimethyl sulfoxide; at 130 ℃; for 18h;

Reference yield: 36.0%

2-{4-[3-methanesulfonyl-1-(4-methoxyphenyl)-7-oxo-1,4,5,7-tetrahydropyrazolo[3,4-c]pyridin-6-yl]phenyl}-2-methylpropionic acid methyl ester (630383-89-0) → 2-{4-[1-(4-methoxypheny)-3-(methylsulfonyl)-7-oxo-1,4,5,7-tetrahydro-6H-pyrazolo[3,4-c]pyridin-6-yl]phenyl}-2-methylpropionamide

Guidance literature:

With ammonia; In ethylene glycol; at 80 ℃; for 18h;

upstream raw materials:

1-(4-methoxyphenyl)-7-oxo-4,5,6,7-tetrahydro-1H-pyrazolo[3, 4-c]pyridine-3-carboxylic acid ethyl ester

2-(4-Iodo-phenyl)-2-methyl-propionic acid methyl ester

1-(4-methoxyphenyl)-3-(methylsulfonyl)-1,4,5,6-tetrahydro-7H-pyrazolo[3,4-c]pyridin-7-one

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