S-Isopropyl O-trimethylsilyl isopropyldithiophosphonate

Base Information

• Chemical Name: S-Isopropyl O-trimethylsilyl isopropyldithiophosphonate
• CAS No.: 131570-89-3
• Molecular Formula: C₉H₂₃OPS₂Si
• Molecular Weight: 270.472
• Mol file: 131570-89-3.mol

Synonyms:S-Isopropyl O-trimethylsilyl isopropyldithiophosphonate

Chemical Property of S-Isopropyl O-trimethylsilyl isopropyldithiophosphonate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of S-Isopropyl O-trimethylsilyl isopropyldithiophosphonate

There total 2 articles about S-Isopropyl O-trimethylsilyl isopropyldithiophosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.6%

N,N,S-triethyl-thiohydroxylamine (32833-97-9) + S,S-diisopropyl O-(trimethylsilyl) phosphorodithioite (127612-42-4) → Trithiophosphoric acid S-ethyl ester S',S''-diisopropyl ester (131570-86-0) + S-Isopropyl O-trimethylsilyl isopropyldithiophosphonate (131570-89-3) + N,N-diethyl-1,1,1-trimethylsilanamine (996-50-9)

Guidance literature:

DOI:10.1007/BF00958273

Reference yield:

N,N-Diethyl-S-isopropylsulfenamide (126989-46-6) + S,S-diisopropyl O-(trimethylsilyl) phosphorodithioite (127612-42-4) → S-Isopropyl O-trimethylsilyl isopropyldithiophosphonate (131570-89-3) + N,N-diethyl-1,1,1-trimethylsilanamine (996-50-9)

Guidance literature:

for 96h; Ambient temperature;

DOI:10.1007/BF00958273

upstream raw materials:

N,N,S-triethyl-thiohydroxylamine

S,S-diisopropyl O-(trimethylsilyl) phosphorodithioite

N,N-Diethyl-S-isopropylsulfenamide