3-[(allylmethylamino)methyl]-4-ethanesulfonylphenylamine

Base Information

Chemical Name:3-[(allylmethylamino)methyl]-4-ethanesulfonylphenylamine
CAS No.:1354567-44-4
Molecular Formula:C₁₃H₂₀N₂O₂S
Molecular Weight:268.38
Hs Code.:

Synonyms:3-[(allylmethylamino)methyl]-4-ethanesulfonylphenylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-[(allylmethylamino)methyl]-4-ethanesulfonylphenylamine

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Technology Process of 3-[(allylmethylamino)methyl]-4-ethanesulfonylphenylamine

There total 5 articles about 3-[(allylmethylamino)methyl]-4-ethanesulfonylphenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1354566-99-6
allylmethyl-(2-ethanesulfonyl-5-nitrobenzyl)amine

: 1354567-44-4
3-[(allylmethylamino)methyl]-4-ethanesulfonylphenylamine

Guidance literature:: With iron; ammonium chloride; In ethanol; water; Reflux;
DOI:10.1021/jm201112g

Reference yield:

: 1354566-87-2
1-chloro-2-(dimethoxymethyl)-4-nitrobenzene

: 1354567-44-4
3-[(allylmethylamino)methyl]-4-ethanesulfonylphenylamine

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / N,N-dimethyl-formamide / 7 h / 70 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane; water / 24 h / 0 - 20 °C

4: sodium tris(acetoxy)borohydride / dichloromethane / 20 °C

5: iron; ammonium chloride / ethanol; water / Reflux

With sodium tris(acetoxy)borohydride; iron; potassium carbonate; ammonium chloride; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm201112g

Reference yield:

: 1354566-89-4
2-dimethoxymethyl-1-ethanesulfonyl-4-nitrobenzene

: 1354567-44-4
3-[(allylmethylamino)methyl]-4-ethanesulfonylphenylamine

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / dichloromethane; water / 24 h / 0 - 20 °C

2: sodium tris(acetoxy)borohydride / dichloromethane / 20 °C

3: iron; ammonium chloride / ethanol; water / Reflux

With sodium tris(acetoxy)borohydride; iron; ammonium chloride; trifluoroacetic acid; In ethanol; dichloromethane; water;
DOI:10.1021/jm201112g